食品研究与开发
食品研究與開髮
식품연구여개발
FOOD RESEARCH AND CEVELOPMENT
2015年
5期
24-28
,共5页
李海平%李艳芳%刘艳则%王迎进
李海平%李豔芳%劉豔則%王迎進
리해평%리염방%류염칙%왕영진
苦参%总酚%响应面分析法%工艺条件
苦參%總酚%響應麵分析法%工藝條件
고삼%총분%향응면분석법%공예조건
Sophora flavescens%total phenol%response surface methodology%process conditions
利用Design-Expert 7.1.6软件Box-Benhnken中心组合试验和响应面分析法优化苦参中总酚的提取工艺条件。在单因素试验的基础上,考察乙醇浓度、超声时间、液料比和超声温度的单一和交互因素对苦参提取率的影响。结果表明:苦参总酚的最佳提取工艺为乙醇浓度44.20%、超声时间29.50 min、液料比32.50∶1(mL/g)、超声温度57.00℃,在此条件下苦参总酚提取率可达4.51%。
利用Design-Expert 7.1.6軟件Box-Benhnken中心組閤試驗和響應麵分析法優化苦參中總酚的提取工藝條件。在單因素試驗的基礎上,攷察乙醇濃度、超聲時間、液料比和超聲溫度的單一和交互因素對苦參提取率的影響。結果錶明:苦參總酚的最佳提取工藝為乙醇濃度44.20%、超聲時間29.50 min、液料比32.50∶1(mL/g)、超聲溫度57.00℃,在此條件下苦參總酚提取率可達4.51%。
이용Design-Expert 7.1.6연건Box-Benhnken중심조합시험화향응면분석법우화고삼중총분적제취공예조건。재단인소시험적기출상,고찰을순농도、초성시간、액료비화초성온도적단일화교호인소대고삼제취솔적영향。결과표명:고삼총분적최가제취공예위을순농도44.20%、초성시간29.50 min、액료비32.50∶1(mL/g)、초성온도57.00℃,재차조건하고삼총분제취솔가체4.51%。
The ultrasonic-assisted extraction process of total phenol from Sophora flavescens was studied using Box-Benhnken center composite design and response surface methodology (RSM). Based on the experiment of single factor, the impacts of ethanol concentration, extraction time, ratio of liquid to solid, extraction temperature and interaction among them on extraction rate of total phenol was studied by RSM. The result suggested that the optimum extraction conditions were as follow:ethanol concentration of 44.20%, extraction time of 29.50 min ratio of liquid to solid of 32.50∶1(mL/g), and extraction temperature of 57.00℃. Under these conditions, the practical yield of total phenol reached to 4.51%.