化学研究
化學研究
화학연구
CHEMICAL RESEARCHES
2015年
2期
158-161
,共4页
张燕菊%许志刚%刘智敏%田世杰%张仙丽
張燕菊%許誌剛%劉智敏%田世傑%張仙麗
장연국%허지강%류지민%전세걸%장선려
灯盏花%槲皮素%真空回流提取%高效液相色谱法
燈盞花%槲皮素%真空迴流提取%高效液相色譜法
등잔화%곡피소%진공회류제취%고효액상색보법
Erigeron Breviscapus%quercetin%reflux extraction under vacuum%high perform-ance liquid chromatograph
云南具有丰富的植物和药物资源,其主要成分的有效提取成为高效利用的关键。本文作者采用真空回流法提取灯盏花中的槲皮素黄酮化合物,优化了提取条件,结合高效液相色谱法对提取产物进行了测定,并与常压回流提取法进行了对照;结合提取后样品的扫描电镜分析,探讨了不同提取方法对提取产物表观结构的影响。结果表明,真空联用提取法优于常压提取法,利用真空负压下的提取可避免黄酮化合物的氧化,提高提取效率。
雲南具有豐富的植物和藥物資源,其主要成分的有效提取成為高效利用的關鍵。本文作者採用真空迴流法提取燈盞花中的槲皮素黃酮化閤物,優化瞭提取條件,結閤高效液相色譜法對提取產物進行瞭測定,併與常壓迴流提取法進行瞭對照;結閤提取後樣品的掃描電鏡分析,探討瞭不同提取方法對提取產物錶觀結構的影響。結果錶明,真空聯用提取法優于常壓提取法,利用真空負壓下的提取可避免黃酮化閤物的氧化,提高提取效率。
운남구유봉부적식물화약물자원,기주요성분적유효제취성위고효이용적관건。본문작자채용진공회류법제취등잔화중적곡피소황동화합물,우화료제취조건,결합고효액상색보법대제취산물진행료측정,병여상압회류제취법진행료대조;결합제취후양품적소묘전경분석,탐토료불동제취방법대제취산물표관결구적영향。결과표명,진공련용제취법우우상압제취법,이용진공부압하적제취가피면황동화합물적양화,제고제취효솔。
Yunnan has abundant resources of plants and herbs ,and the efficient applications of those plants and herbs naturally highly depend on the efficient extraction of the main compo‐nents .Thus a vacuum reflux route was established to extract quercetion flavonoid from Eriger‐on Breviscapus .The extraction conditions were optimized .The extracted products were deter‐mined by high‐performance liquid chromatograph (HPLC) ,while the extraction efficiency of the present route was compared with that of conventional atmosphere solvent reflux method . Moreover ,the effects of different extraction methods on the appearance of the extracted prod‐ucts were investigated based on scanning electron microscopic observations .It was found that the vacuum extraction method is superior over atmosphere solvent reflux method ,which is be‐cause the reflux extraction under vacuum favors to prevent flavonoids from oxidation and in‐crease the extraction efficiency as well .