超硬材料工程
超硬材料工程
초경재료공정
SUPERHARD MATERIAL ENGINEERING
2015年
2期
11-14
,共4页
刘文平%秦建新%秦海青%林峰%雷晓旭
劉文平%秦建新%秦海青%林峰%雷曉旭
류문평%진건신%진해청%림봉%뢰효욱
纳米金刚石%分散%激光粒度%温度%浓度
納米金剛石%分散%激光粒度%溫度%濃度
납미금강석%분산%격광립도%온도%농도
nano diamond%dispersion%laser particle size%temperature%concentration
结合场发射扫描电镜和纳米激光粒度仪研究了型号 w0.5金刚石的形貌及其在水溶液中分散稳定性的影响。FE-SEM 表明型号 w0.5的金刚石为粒度在几百纳米,形状不规则的纳米颗粒。激光粒度测试表明随着金刚石浓度从0.01 wt.%增加到0.4 wt.%,纳米金刚石的分散粒径先减小后增大,浓度为0.1 wt.%,分散效果最好,中粒径为232.3nm。随着测试温度的升高,分散的纳米颗粒再次团聚,在15℃和25℃时,测试分散粒径最佳。
結閤場髮射掃描電鏡和納米激光粒度儀研究瞭型號 w0.5金剛石的形貌及其在水溶液中分散穩定性的影響。FE-SEM 錶明型號 w0.5的金剛石為粒度在幾百納米,形狀不規則的納米顆粒。激光粒度測試錶明隨著金剛石濃度從0.01 wt.%增加到0.4 wt.%,納米金剛石的分散粒徑先減小後增大,濃度為0.1 wt.%,分散效果最好,中粒徑為232.3nm。隨著測試溫度的升高,分散的納米顆粒再次糰聚,在15℃和25℃時,測試分散粒徑最佳。
결합장발사소묘전경화납미격광립도의연구료형호 w0.5금강석적형모급기재수용액중분산은정성적영향。FE-SEM 표명형호 w0.5적금강석위립도재궤백납미,형상불규칙적납미과립。격광립도측시표명수착금강석농도종0.01 wt.%증가도0.4 wt.%,납미금강석적분산립경선감소후증대,농도위0.1 wt.%,분산효과최호,중립경위232.3nm。수착측시온도적승고,분산적납미과립재차단취,재15℃화25℃시,측시분산립경최가。
Morphology and dispersion stability of w0.5 type diamond in aqueous solution have been reseached by both of field emission scanning electron microscopy (FESEM)and nano laser granulometer.FESEM result shows that the w0.5 type diamond consists of ir-regular shaped nano particles of a few hundred nanometers.Laser particle size test shows when the diamond concentration has been increased from 0.01 wt.% to 0.4 wt.%,the dispersion particle size of the nano diamond decreases first and then increases.The disper-sion effect is the best with a median particle size of 232.3nm when concentration is at 0.1 wt.%.With the testing temperature rises,the dispersed nano particles reunite again. The dispersion particle size is the best at the temperature of 15℃ and 25℃.