CAJ | 학술논문

目的：建立气相色谱法玫瑰麝香油色谱图像，为其质量控制提供依据。方法：采用毛细管柱气相色谱法，用DB-FFAP（30m×0.25mm×0.25um）柱，以硝基对苯二酸改性的聚乙二醇为固定相；进样口温度为250℃，分流比为100∶1，程序升温：初始为70℃，保持5min，以5℃·min-1升温至220℃，保持5min；载气为氮气，流量为1.0ml·min-1；以FID为检测器，检测器温度为280℃；进样量为0.2μl。结果：建立玫瑰麝香油气相色谱图像，并设定各主要成分低限，D-柠檬萜为2.3%，芳樟醇为2.7%，乙酸苄酯为5.2%，乙酸香叶酯为0.8%，香叶醇为14.0%，香豆素为9.8%。结论：本方法简便、可靠，可用于评价玫瑰麝香油的质量，亦可为其他天然辅料的质量控制提供思路。
목적：건립기상색보법매괴사향유색보도상，위기질량공제제공의거。방법：채용모세관주기상색보법，용DB-FFAP（30m×0.25mm×0.25um）주，이초기대분이산개성적취을이순위고정상；진양구온도위250℃，분류비위100∶1，정서승온：초시위70℃，보지5min，이5℃·min-1승온지220℃，보지5min；재기위담기，류량위1.0ml·min-1；이FID위검측기，검측기온도위280℃；진양량위0.2μl。결과：건립매괴사향유기상색보도상，병설정각주요성분저한，D-저몽첩위2.3%，방장순위2.7%，을산변지위5.2%，을산향협지위0.8%，향협순위14.0%，향두소위9.8%。결론：본방법간편、가고，가용우평개매괴사향유적질량，역가위기타천연보료적질량공제제공사로。
Objective : To establish a chromatographyprofile for rose musk essential oil. Method:A capillary gas chromatographic methodwas carried out, DB-FFAP capillary column (30m×0.25mm×0.25μm)was usedwith the injection port temperature of 250℃, and the split ratio wasset at 100∶1. The column temperaturewas raised by temperature programming.The initialcolumn temperature was 70℃, maintained for 5min, raised to 220℃with a rate of 5℃·min-1,maintained for 5 min.The carry gas was nitrogen and the flow rate of carry gas was 1.0ml·min-1. The temperature of FIDwas set at 280℃, and the samplevolume was setat0.2ul.Results:the Chromatography profile of Rose Musk Essential Oils by GC was established ,and the limited of compositions were set , D-Limonene is 2.3%,Linalool is 2.7%, Benzyl Acetate is 5.2%, Geranyl Acetate is 0.8% ,Geraniol is 14.0%, and Coumarin is 9.8%.Conclusion:This method is simpleand reliable, and can be used to evaluate the quality of Rose musk, and also can provide ideas of quality control for other natural excipients.