环境科学导刊
環境科學導刊
배경과학도간
ENVIRONMENTAL SCIENCE SURVEY
2015年
3期
98-101
,共4页
徐国津%张妍%胡财平%樊颖果%赵倩%李琦
徐國津%張妍%鬍財平%樊穎果%趙倩%李琦
서국진%장연%호재평%번영과%조천%리기
固定污染源废气%FAAS%ICP -AES%铅%对比研究
固定汙染源廢氣%FAAS%ICP -AES%鉛%對比研究
고정오염원폐기%FAAS%ICP -AES%연%대비연구
stationary source emission%Lead%Comparison study
以石英纤维滤筒采样,采用硝酸-氢氟酸消解体系,建立了火焰原子吸收光谱法和电感耦合等离子体原子发射光谱法测定固定污染源废气中铅的分析方法。分别对两种方法的波长选择、干扰因素、标准曲线、检出限、准确度和精密度等方面进行了对比研究,并对两种方法的测定结果进行 t 检验。结果表明,两种方法无显著性差异,均可用于固定污染源废气中铅的含量测定。
以石英纖維濾筒採樣,採用硝痠-氫氟痠消解體繫,建立瞭火燄原子吸收光譜法和電感耦閤等離子體原子髮射光譜法測定固定汙染源廢氣中鉛的分析方法。分彆對兩種方法的波長選擇、榦擾因素、標準麯線、檢齣限、準確度和精密度等方麵進行瞭對比研究,併對兩種方法的測定結果進行 t 檢驗。結果錶明,兩種方法無顯著性差異,均可用于固定汙染源廢氣中鉛的含量測定。
이석영섬유려통채양,채용초산-경불산소해체계,건립료화염원자흡수광보법화전감우합등리자체원자발사광보법측정고정오염원폐기중연적분석방법。분별대량충방법적파장선택、간우인소、표준곡선、검출한、준학도화정밀도등방면진행료대비연구,병대량충방법적측정결과진행 t 검험。결과표명,량충방법무현저성차이,균가용우고정오염원폐기중연적함량측정。
The quartz fiber filter tube for sampling and nitric acid -hydrofluoric acid digestion system were used in order to develop two methods of flame atomic absorption spectrometry and inductively coupled plasma atomic emis-sion spectrometry to test Lead in stationary sources.Theselectionofwavelength,interference factors,standard curves,the detection limits,accuracy and precision of two methods were compared.Furthermore,a t -test was carried out for the results of the two methods.The results showed that there were no significant differences in the two methods,which indicated that both methods could be used for the determination of lead in stationary