食品安全质量检测学报
食品安全質量檢測學報
식품안전질량검측학보
FOOD SAFETY AND QUALITY DETECTION TECHNOLOGY
2015年
5期
1913-1918
,共6页
陈彩云%蔡伟江%陈宏壁%林贤邦
陳綵雲%蔡偉江%陳宏壁%林賢邦
진채운%채위강%진굉벽%림현방
高效液相色谱法%保健食品%硫酸软骨素%含量测定?
高效液相色譜法%保健食品%硫痠軟骨素%含量測定?
고효액상색보법%보건식품%류산연골소%함량측정?
high?performance?liquid?chromatography%health?foods%chondroitin?sulfate%determination??
目的:建立一种快速、简便测定保健食品中硫酸软骨素的液相色谱方法,并进行方法学研究。方法样品经过前处理,以乙腈和0.005 mol/L戊烷磺酸钠溶液为流动相,等度洗脱,经Diamonsil C18柱分离,于192 nm波长检测。结果用本方法进行检测,能很好地分离硫酸软骨素,在浓度0.008 mg/mL~0.04 mg/mL之间呈现良好的线性关系,方法的相关系数可达1.000,平均回收率在98.5%~100.0%之间,相对标准偏差为0.6%。结论采用该方法能测定保健食品中硫酸软骨素,耗时短、操作简便、准确、重现性好,分离效果明显,可在实验室推广。
目的:建立一種快速、簡便測定保健食品中硫痠軟骨素的液相色譜方法,併進行方法學研究。方法樣品經過前處理,以乙腈和0.005 mol/L戊烷磺痠鈉溶液為流動相,等度洗脫,經Diamonsil C18柱分離,于192 nm波長檢測。結果用本方法進行檢測,能很好地分離硫痠軟骨素,在濃度0.008 mg/mL~0.04 mg/mL之間呈現良好的線性關繫,方法的相關繫數可達1.000,平均迴收率在98.5%~100.0%之間,相對標準偏差為0.6%。結論採用該方法能測定保健食品中硫痠軟骨素,耗時短、操作簡便、準確、重現性好,分離效果明顯,可在實驗室推廣。
목적:건립일충쾌속、간편측정보건식품중류산연골소적액상색보방법,병진행방법학연구。방법양품경과전처리,이을정화0.005 mol/L무완광산납용액위류동상,등도세탈,경Diamonsil C18주분리,우192 nm파장검측。결과용본방법진행검측,능흔호지분리류산연골소,재농도0.008 mg/mL~0.04 mg/mL지간정현량호적선성관계,방법적상관계수가체1.000,평균회수솔재98.5%~100.0%지간,상대표준편차위0.6%。결론채용해방법능측정보건식품중류산연골소,모시단、조작간편、준학、중현성호,분리효과명현,가재실험실추엄。
Objective To investigate a quick and simple method for determination of chondroitin sulfate in health foods by high performance liquid chromatography (HPLC). Methods Samples were treated using 0.005 mol/L pentane solution of sodium-acetonitrile as mobile phase with isocratic elution, separated on diamonsil C18 column, and detected at 192 nm wavelength. Results Chondroitin sulfate could be separated well by this method. It had a good linear relationship within 0.008~0.04 mg/mL (r=1.000), the average recoveries was 98.5%~100.0%, and the RSD was 0.6%. Conclusion The method can be used for determination of chondroitin sulfate in health foods, it is quick, simple and accurate, and has a good reproducibility and clear separation, which can be popularized in the laboratory.