药学实践杂志
藥學實踐雜誌
약학실천잡지
THE JOURNAL OF PHARMACEUTICAL PRACTICE
2015年
3期
255-257
,共3页
陈旭%楼永明%黄爱文%宋洪涛
陳旭%樓永明%黃愛文%宋洪濤
진욱%루영명%황애문%송홍도
薄荷水%质量控制%薄层色谱法%气相色谱法%薄荷脑
薄荷水%質量控製%薄層色譜法%氣相色譜法%薄荷腦
박하수%질량공제%박층색보법%기상색보법%박하뇌
peppermint water%quality standard%thin layer chromatography%gas chromatography%mentholum
目的:完善薄荷水的质量控制方法。方法采用薄层色谱法鉴别薄荷水中的薄荷素油,用气相色谱法测定薄荷水中薄荷脑的含量。结果薄层色谱法鉴别专属性强;气相色谱法中,薄荷脑线性范围为5.0~80.0μg/ml(r=0.9999),平均回收率为103.16%,RSD为1.81%。结论该法操作简便,结果准确,灵敏度高,重复性好,可有效地控制薄荷水的质量。
目的:完善薄荷水的質量控製方法。方法採用薄層色譜法鑒彆薄荷水中的薄荷素油,用氣相色譜法測定薄荷水中薄荷腦的含量。結果薄層色譜法鑒彆專屬性彊;氣相色譜法中,薄荷腦線性範圍為5.0~80.0μg/ml(r=0.9999),平均迴收率為103.16%,RSD為1.81%。結論該法操作簡便,結果準確,靈敏度高,重複性好,可有效地控製薄荷水的質量。
목적:완선박하수적질량공제방법。방법채용박층색보법감별박하수중적박하소유,용기상색보법측정박하수중박하뇌적함량。결과박층색보법감별전속성강;기상색보법중,박하뇌선성범위위5.0~80.0μg/ml(r=0.9999),평균회수솔위103.16%,RSD위1.81%。결론해법조작간편,결과준학,령민도고,중복성호,가유효지공제박하수적질량。
Objective To consummate a method of quality control of peppermint water .Methods Thin layer chromatog-raphy was used for the identification of peppermint oil .Gas chromatography was used for the determination of mentholum . Results The identification of peppermint oil was highly specific by TLC .The linear range of mentholum was from 5 .0-80 .0 μg/ml ,r=0 .999 9 .The average recovery of mentholum was 103 .16% and RSD was 1 .81% .Conclusion These methods were easy to operate with accurate results ,which washigh sensitivity andgoodrepeatability .This quality standard could effective-ly control the quality of peppermint water .