工程科学学报
工程科學學報
공정과학학보
Journal of University of Science and Technology Beijing
2015年
5期
75-80
,共6页
镍基高温合金%单晶%蠕变断裂%形貌
鎳基高溫閤金%單晶%蠕變斷裂%形貌
얼기고온합금%단정%연변단렬%형모
nickel base superalloys%single crystals%creep fracture%morphology
研究了[011]取向的镍基单晶高温合金在750~980℃温度范围和200~680 MPa应力下的蠕变断裂特征。在扫描电镜上对各种实验状态下的蠕变断口和纵向剖面进行了详细观察。研究发现:在低温750℃和中温870℃不同初始蠕变应力条件下,枝晶间区亚晶界处不规则γ'/γ界面是裂纹主要萌生场所,这些已萌生的裂纹在与外加应力轴垂直的(011)面上沿<110>和<100>两个方向扩展;980℃不同初始应力条件下,裂纹主要在合金中显微疏松孔洞处萌生,沿与外应力轴垂直的方向扩展。观察750℃和870℃不同应力状态蠕变试样的纵向剖面,对亚晶界区不规则γ'相面积分数的测量和计算表明,用面积分数表征该合金[011]取向在中低温状态下的蠕变损伤程度是可行的。
研究瞭[011]取嚮的鎳基單晶高溫閤金在750~980℃溫度範圍和200~680 MPa應力下的蠕變斷裂特徵。在掃描電鏡上對各種實驗狀態下的蠕變斷口和縱嚮剖麵進行瞭詳細觀察。研究髮現:在低溫750℃和中溫870℃不同初始蠕變應力條件下,枝晶間區亞晶界處不規則γ'/γ界麵是裂紋主要萌生場所,這些已萌生的裂紋在與外加應力軸垂直的(011)麵上沿<110>和<100>兩箇方嚮擴展;980℃不同初始應力條件下,裂紋主要在閤金中顯微疏鬆孔洞處萌生,沿與外應力軸垂直的方嚮擴展。觀察750℃和870℃不同應力狀態蠕變試樣的縱嚮剖麵,對亞晶界區不規則γ'相麵積分數的測量和計算錶明,用麵積分數錶徵該閤金[011]取嚮在中低溫狀態下的蠕變損傷程度是可行的。
연구료[011]취향적얼기단정고온합금재750~980℃온도범위화200~680 MPa응력하적연변단렬특정。재소묘전경상대각충실험상태하적연변단구화종향부면진행료상세관찰。연구발현:재저온750℃화중온870℃불동초시연변응력조건하,지정간구아정계처불규칙γ'/γ계면시렬문주요맹생장소,저사이맹생적렬문재여외가응력축수직적(011)면상연<110>화<100>량개방향확전;980℃불동초시응력조건하,렬문주요재합금중현미소송공동처맹생,연여외응력축수직적방향확전。관찰750℃화870℃불동응력상태연변시양적종향부면,대아정계구불규칙γ'상면적분수적측량화계산표명,용면적분수표정해합금[011]취향재중저온상태하적연변손상정도시가행적。
The creep fracture behavior of a [011] oriented single crystal nickel base superalloy was investigated in the tempera-ture range of 750 to 980℃ and the stress scope of 200 to 680 MPa. The fracture surfaces and longitudinal sections of crept specimens were examined by scanning electron microscopy ( SEM) . It is found that under different initial stresses at 750℃ and 870℃, creep cracks seem always to initiate at theγ'/γinterface on the interdendritic sub-boundary and propagate along the sub-boundary trace, and their cleavage planes expand along<110> and<100> on the (011) plane. But under different stresses at 980℃, creep cracks initiate at inherent casting pores and slowly propagate perpendicular to the axis of stress applied up to the final fast fracture. After observing the longitudinal sections of specimens crept under different stresses at 750℃ and 870℃, it is feasible for the area fraction of irregularγ' phase in the sub-boundary to characterize the creep damage level before collapsing of the superalloy along the [011] direction at the moderated and low temperatures.