岩矿测试
巖礦測試
암광측시
ROCK AND MINERAL ANALYSIS
2015年
3期
278-285
,共8页
王羽%金婵%汪丽华%王建强%姜政%王彦飞%普洁
王羽%金嬋%汪麗華%王建彊%薑政%王彥飛%普潔
왕우%금선%왕려화%왕건강%강정%왕언비%보길
微观孔隙结构%氩离子抛光%扫描电子显微镜%四川盆地%九老洞组页岩
微觀孔隙結構%氬離子拋光%掃描電子顯微鏡%四川盆地%九老洞組頁巖
미관공극결구%아리자포광%소묘전자현미경%사천분지%구로동조혈암
microscopic pore structure%Ar-ion milling%Scanning Electron Microscope%Sichuan Basin%Jiulaodong Formation Shale
微观孔隙结构是页岩储层研究的重点,而扫描电镜方法无法识别机械抛光中由于页岩硬度差异所造成的不规则形貌。本文利用氩离子抛光-扫描电镜方法对四川威远区块九老洞组页岩进行研究,发现了三种孔隙类型:①无机孔以粒间孔和黏土矿物层间孔为主,同时发育晶间孔和生物孔,孔径主体100~500 nm;②有机孔受控于热成熟度或有机黏土复合体,孔径范围数十纳米至数微米;③微裂缝包括成岩收缩裂缝、高压碎裂缝、构造裂缝和人为裂缝,缝宽数微米,缝长数微米至数十微米。研究表明无机孔和微裂缝是九老洞组页岩气的主要储集空间。
微觀孔隙結構是頁巖儲層研究的重點,而掃描電鏡方法無法識彆機械拋光中由于頁巖硬度差異所造成的不規則形貌。本文利用氬離子拋光-掃描電鏡方法對四川威遠區塊九老洞組頁巖進行研究,髮現瞭三種孔隙類型:①無機孔以粒間孔和黏土礦物層間孔為主,同時髮育晶間孔和生物孔,孔徑主體100~500 nm;②有機孔受控于熱成熟度或有機黏土複閤體,孔徑範圍數十納米至數微米;③微裂縫包括成巖收縮裂縫、高壓碎裂縫、構造裂縫和人為裂縫,縫寬數微米,縫長數微米至數十微米。研究錶明無機孔和微裂縫是九老洞組頁巖氣的主要儲集空間。
미관공극결구시혈암저층연구적중점,이소묘전경방법무법식별궤계포광중유우혈암경도차이소조성적불규칙형모。본문이용아리자포광-소묘전경방법대사천위원구괴구로동조혈암진행연구,발현료삼충공극류형:①무궤공이립간공화점토광물층간공위주,동시발육정간공화생물공,공경주체100~500 nm;②유궤공수공우열성숙도혹유궤점토복합체,공경범위수십납미지수미미;③미렬봉포괄성암수축렬봉、고압쇄렬봉、구조렬봉화인위렬봉,봉관수미미,봉장수미미지수십미미。연구표명무궤공화미렬봉시구로동조혈암기적주요저집공간。
Microscopic pore structure is the key to studying shale gas reservoirs.Traditional Scanning Electron Microscope cannot be used to identify topographic irregularities caused by differential hardness of components during mechanical polishing.Microscopic pore structures of Jiulaodong formation shale in the Weiyuan area of the Sichuan basin were investigated using scanning electron microscope coupled with an Ar-ion milling technique.Three types of pores were identified:(1 )mineral matrix pores (pore diameters are mostly 100 -500 nm),mainly including interparticle pores and intraplatelet pores within clay aggregates,and intercrystalline pores within pyrite /anatase and biological pores;(2 )organic matter pores (pore diameters range from tens of nanometers to several micrometers),either controlled by thermal evolution of kerogen or clay minerals coated by organic matter;(3)micro fractures (with length of dozens of micrometers and width of a few micrometers),including shrinkage fracture,tectonic fracture,overpressure fracture and artificial fracture.In conclusion,micro-nano pores in Jiulaodong shale are mainly composed of mineral matrix pores and micro fractures which provide the main storage space and flow channel for shale gas.