中国土壤与肥料
中國土壤與肥料
중국토양여비료
SOIL AND FERTILIZER SCIENCES IN CHINA
2015年
3期
111-115
,共5页
李桂花%叶小兰%吕子古%杨森%温云杰%刘云霞%汪洪
李桂花%葉小蘭%呂子古%楊森%溫雲傑%劉雲霞%汪洪
리계화%협소란%려자고%양삼%온운걸%류운하%왕홍
杜马斯催化燃烧法%全自动凯氏定氮仪%土壤全氮%元素分析仪
杜馬斯催化燃燒法%全自動凱氏定氮儀%土壤全氮%元素分析儀
두마사최화연소법%전자동개씨정담의%토양전담%원소분석의
automated micro Kjeldahl method%Dumas method%soil total nitrogen%elemental analyzer
土壤全氮含量反映土壤中氮循环的状况,是评价土壤肥力与土壤资源的一项重要指标。选择黑土和潮土,分别利用元素分析仪(杜马斯催化燃烧法)和全自动凯氏定氮仪(凯氏消煮蒸馏法)测定土壤全氮含量,以揭示两种仪器测定结果的可比性,每个样品每种方法重复测定5次。结果表明:元素分析仪和全自动凯氏定氮仪测定的黑土全氮含量(平均值±标准偏差)分别为(1.37±0.01) g/ kg 和(1.36±0.01) g/ kg,潮土全氮含量分别为(0.75±0.02) g/ kg 和(0.78±0.03) g/ kg, t 检测表明,两种仪器测定结果之间无显著性差异。两种仪器土壤全氮测定结果精确度均较高,稳定性较好,相对标准偏差均小于5%。本研究结果可为采用仪器方法测定土壤全氮含量及评价土壤氮库变化提供参考。
土壤全氮含量反映土壤中氮循環的狀況,是評價土壤肥力與土壤資源的一項重要指標。選擇黑土和潮土,分彆利用元素分析儀(杜馬斯催化燃燒法)和全自動凱氏定氮儀(凱氏消煮蒸餾法)測定土壤全氮含量,以揭示兩種儀器測定結果的可比性,每箇樣品每種方法重複測定5次。結果錶明:元素分析儀和全自動凱氏定氮儀測定的黑土全氮含量(平均值±標準偏差)分彆為(1.37±0.01) g/ kg 和(1.36±0.01) g/ kg,潮土全氮含量分彆為(0.75±0.02) g/ kg 和(0.78±0.03) g/ kg, t 檢測錶明,兩種儀器測定結果之間無顯著性差異。兩種儀器土壤全氮測定結果精確度均較高,穩定性較好,相對標準偏差均小于5%。本研究結果可為採用儀器方法測定土壤全氮含量及評價土壤氮庫變化提供參攷。
토양전담함량반영토양중담순배적상황,시평개토양비력여토양자원적일항중요지표。선택흑토화조토,분별이용원소분석의(두마사최화연소법)화전자동개씨정담의(개씨소자증류법)측정토양전담함량,이게시량충의기측정결과적가비성,매개양품매충방법중복측정5차。결과표명:원소분석의화전자동개씨정담의측정적흑토전담함량(평균치±표준편차)분별위(1.37±0.01) g/ kg 화(1.36±0.01) g/ kg,조토전담함량분별위(0.75±0.02) g/ kg 화(0.78±0.03) g/ kg, t 검측표명,량충의기측정결과지간무현저성차이。량충의기토양전담측정결과정학도균교고,은정성교호,상대표준편차균소우5%。본연구결과가위채용의기방법측정토양전담함량급평개토양담고변화제공삼고。
Nitrogen (N) is one of the most important elements for plant nutrition. It is necessary to apply reliable methods for N determination in soils. Among the different methods of total N determination in soils, the Kjeldahl method (wet oxidation) and the elemental analyzer (Dumas dry combustion method) are more frequently used. In this study, black soil was sampled from Heilongjiang provinces in Northeast China and calcareous fluvo-aquic soil sample was from Shandong provinces in North China Plain. The objective of this study was to compare soil total N contents determined by a CNS elemental analyzer (vario PYRO cube, Elementar Analysensysteme GmbH) and an automated Kjeldahl N determination instrument (BüCHI Labortech-nik AG). The results showed that total N contents of black soil samples measured by the elemental analyzer and the automated micro-Kjeldahl method were (1. 37 ± 0. 01) g/ kg and (1. 36 ± 0. 01) g/ kg (mean ± SD), respectively. The N contents of fluvo-aquic soil samples were (0. 75 ± 0. 02) g/ kg through the elemental analyzer method and (0. 78 ± 0. 03) g/ kg by the automated Kjeldahl method. The t test found there was no significant difference of soil N measured by two kinds of instruments. Both methods for soil N measurement had a high precision with relative standard deviation (RSD) less than 5% .