CAJ | 학술논문

采用 Hydra C 自动固体测汞仪，结合应用还原催化和金汞齐富集技术，建立了测定载金树脂物料中痕量汞的固体进样-冷原子吸收法。标准汞溶液在0.0~100.0 ng/ mL 浓度范围内呈较好的线性关系，回归系数 r =0.9995，方法检出限为0.2μg/ kg，测定结果的相对标准偏差为1.94%，与原子荧光法比较，两种方法无显著性差异。本法操作简单、快速、灵敏，适用于载金树脂中汞含量的检测。
채용 Hydra C 자동고체측홍의，결합응용환원최화화금홍제부집기술，건립료측정재금수지물료중흔량홍적고체진양-랭원자흡수법。표준홍용액재0.0~100.0 ng/ mL 농도범위내정교호적선성관계，회귀계수 r =0.9995，방법검출한위0.2μg/ kg，측정결과적상대표준편차위1.94%，여원자형광법비교，량충방법무현저성차이。본법조작간단、쾌속、령민，괄용우재금수지중홍함량적검측。
To develop a method on determination of mercury in gold loaded resin material by solid sam-pling-cold atomic absorption spectrometry. The method use Hydra C automatic solid mercury analyzer combined with the application of gold amalgam reduction catalysis and enrichment technology. Mercury standard solution in the 0. 0 ~ 100. 0 ng / mL concentration range was a good linear relationship,the re-gression coefficient r = 0. 999 5,the detection limit was 0. 2 μg / kg,measured relative standard deviation was 1. 94% ,and with atomic fluorescence comparison,the two methods was no significant difference. The method is simple,rapid,sensitive and suitable for the detection of mercury in gold-resin content.