CAJ | 학술논문

建立了检测水产品中石油烃残留的分析方法。样品与过量的碱液在无水乙醇环境下，40℃水浴避光振摇5 h，再经二氯甲烷萃取、负压蒸干、脱芳石油醚溶解，荧光分光光度法测定。结果表明，油标液在0．0～10．0μg ／ml 线性关系良好，相关系数0．9996，检出限为0．85 mg ／kg，添加质量浓度5．0～20．0 mg ／kg 时，样品回收率在91．5％～97．9％之间。该方法与目前我国海洋生物中石油烃的检测方法 GB17378．6-2007相比，节省时间，且皂化充分，检测结果准确度好，精密度高，适用于水产品中石油烃含量的检测。
건립료검측수산품중석유경잔류적분석방법。양품여과량적감액재무수을순배경하，40℃수욕피광진요5 h，재경이록갑완췌취、부압증간、탈방석유미용해，형광분광광도법측정。결과표명，유표액재0．0～10．0μg ／ml 선성관계량호，상관계수0．9996，검출한위0．85 mg ／kg，첨가질량농도5．0～20．0 mg ／kg 시，양품회수솔재91．5％～97．9％지간。해방법여목전아국해양생물중석유경적검측방법 GB17378．6-2007상비，절성시간，차조화충분，검측결과준학도호，정밀도고，괄용우수산품중석유경함량적검측。
Determination of fluorescence spectrophotometry is established analysis methods of petroleum hydro-carbon residues in aquatic products.Samples and excessive alkali liquor under the environment of anhydrous ethanol,40 ℃ water bath avoid light vibration wave five hours,fully by the methylene chloride extraction after saponification,negative pressure dry,aromatic petroleum ether dissolved,fluorescence spectrophotometry.Re-sults show that the oil standard fluid in 0.0 ~ 10.0 ng /ml linear relationship is good,the correlation coeffi-cient of 0.9996,the detection limit of 0.85 mg /kg,added mass concentration is 5.0 ~20.0 mg /kg,recov-ery is between 91 .5% ~97.9%.Compare to GB17378.6-2007,the method saves time,saponification,ac-curacy of test results is good,high precision,suitable for detection of petroleum hydrocarbon content in aquat-ic products.