固体火箭技术
固體火箭技術
고체화전기술
JOURNAL OF SOLID ROCKET TECHNOLOGY
2015年
3期
445-450
,共6页
李林杰%方国东%易法军%梁军
李林傑%方國東%易法軍%樑軍
리림걸%방국동%역법군%량군
高硅氧/酚醛复合材料%体积烧蚀%DIC方法%变形场%表面形貌分析
高硅氧/酚醛複閤材料%體積燒蝕%DIC方法%變形場%錶麵形貌分析
고규양/분철복합재료%체적소식%DIC방법%변형장%표면형모분석
silica/phenolic composites%volume ablation%DIC method%deformation field%surface morphology analysis
通过非接触式高温变形测量系统,对高硅氧/酚醛防/隔热复合材料在单侧热流载荷作用下的温度和全场高温变形进行了精确测量,并对试样体积烧蚀后的表面微观形貌进行分析。实验结果表明,利用陶瓷板在1000℃左右对高硅氧/酚醛复合材料试件辐射加热200 s后,通过测量发现距离加热面12.62 mm处热电偶温度峰值为259℃,从而说明高硅氧/酚醛复合材料具有优良的防/隔热性能。通过DIC方法测得试样加热200 s后沿加热方向的最大位移为0.18 mm,且沿着试样加热方向位移呈现出逐渐递减的规律。通过对材料烧蚀后表面形貌微观观测和分析,发现在试样加热面上出现了凹凸不平的烧蚀坑,并出现了一层很薄的高硅氧纤维高温熔融后的硅氧化合物颗粒结晶状物质。
通過非接觸式高溫變形測量繫統,對高硅氧/酚醛防/隔熱複閤材料在單側熱流載荷作用下的溫度和全場高溫變形進行瞭精確測量,併對試樣體積燒蝕後的錶麵微觀形貌進行分析。實驗結果錶明,利用陶瓷闆在1000℃左右對高硅氧/酚醛複閤材料試件輻射加熱200 s後,通過測量髮現距離加熱麵12.62 mm處熱電偶溫度峰值為259℃,從而說明高硅氧/酚醛複閤材料具有優良的防/隔熱性能。通過DIC方法測得試樣加熱200 s後沿加熱方嚮的最大位移為0.18 mm,且沿著試樣加熱方嚮位移呈現齣逐漸遞減的規律。通過對材料燒蝕後錶麵形貌微觀觀測和分析,髮現在試樣加熱麵上齣現瞭凹凸不平的燒蝕坑,併齣現瞭一層很薄的高硅氧纖維高溫鎔融後的硅氧化閤物顆粒結晶狀物質。
통과비접촉식고온변형측량계통,대고규양/분철방/격열복합재료재단측열류재하작용하적온도화전장고온변형진행료정학측량,병대시양체적소식후적표면미관형모진행분석。실험결과표명,이용도자판재1000℃좌우대고규양/분철복합재료시건복사가열200 s후,통과측량발현거리가열면12.62 mm처열전우온도봉치위259℃,종이설명고규양/분철복합재료구유우량적방/격열성능。통과DIC방법측득시양가열200 s후연가열방향적최대위이위0.18 mm,차연착시양가열방향위이정현출축점체감적규률。통과대재료소식후표면형모미관관측화분석,발현재시양가열면상출현료요철불평적소식갱,병출현료일층흔박적고규양섬유고온용융후적규양화합물과립결정상물질。
The temperature and full?field high temperature deformation of silica/phenolic composites under unilateral thermal flux were measured accurately by non?contact high temperature deformation testing systems. The surface morphology of specimens af?ter volume ablative experiment was analyzed. It is found that the temperature peak of thermocouple was 259 ℃ when the distance from the heated surface was 12.62 mm after 200 s radiation heating on the silica/phenolic composites specimen by ceramic slab un?der 1 000 ℃. It is shown that the silica/phenolic composites have good thermal protection and insulation performances. The maxi?mum displacement along the heating direction of specimen detected by DIC method is 0.18 mm after heating 200 s, and decreases gradually along the heating direction. After the analysis of ablative surface morphology of specimens, the heating surface of specimen appears uneven ablation pits. Crystalline silicon oxide particles are adsorbed on a thin layer of silica fiber after high temperature melting of silica fiber.