中国烟草科学
中國煙草科學
중국연초과학
CHINESE TOBACCO SCIENCE
2015年
2期
8-13
,共6页
赵会纳%蔡凯%雷波%武圣江%任竹%向章敏%潘文杰%姚珊珊%蔡斌
趙會納%蔡凱%雷波%武聖江%任竹%嚮章敏%潘文傑%姚珊珊%蔡斌
조회납%채개%뢰파%무골강%임죽%향장민%반문걸%요산산%채빈
烤烟%顶空固相微萃取-全二维飞行时间质谱联用法%烘烤%品种%中性致香物质
烤煙%頂空固相微萃取-全二維飛行時間質譜聯用法%烘烤%品種%中性緻香物質
고연%정공고상미췌취-전이유비행시간질보련용법%홍고%품충%중성치향물질
flue-cured tobacco%HS-SPME-GC×GC-TOFMS%curing%cultivar%neutral aroma compound
为探求烘烤过程对烤烟中性致香物质的影响,采用顶空固相微萃取-全二维飞行时间质谱联用法和半叶法研究了K326和南江3号烟叶中性致香物质种类、含量及其比例在烘烤前后的差异。结果表明:(1)多种香气物质在烘烤过程中发生了转化,有19种香气物质在烤后烟叶未检测到,但增加了36种香气物质。(2)烘烤后香气物质总量显著增加,且不同品种烤烟香气物质转化程度不同,K326的香气物质总量(不含新植二烯)显著高于南江3号。(3)烘烤后西柏烷类降解产物占中性致香物质总量的比例明显降低,而苯丙氨酸降解产物和类胡萝卜素降解产物所占比例明显提高。在烘烤过程中损失了醛、醇和酯类等19种香气物质,产生了类胡萝卜素降解产物、棕色化反应产物等36种香气物质。
為探求烘烤過程對烤煙中性緻香物質的影響,採用頂空固相微萃取-全二維飛行時間質譜聯用法和半葉法研究瞭K326和南江3號煙葉中性緻香物質種類、含量及其比例在烘烤前後的差異。結果錶明:(1)多種香氣物質在烘烤過程中髮生瞭轉化,有19種香氣物質在烤後煙葉未檢測到,但增加瞭36種香氣物質。(2)烘烤後香氣物質總量顯著增加,且不同品種烤煙香氣物質轉化程度不同,K326的香氣物質總量(不含新植二烯)顯著高于南江3號。(3)烘烤後西柏烷類降解產物佔中性緻香物質總量的比例明顯降低,而苯丙氨痠降解產物和類鬍蘿蔔素降解產物所佔比例明顯提高。在烘烤過程中損失瞭醛、醇和酯類等19種香氣物質,產生瞭類鬍蘿蔔素降解產物、棕色化反應產物等36種香氣物質。
위탐구홍고과정대고연중성치향물질적영향,채용정공고상미췌취-전이유비행시간질보련용법화반협법연구료K326화남강3호연협중성치향물질충류、함량급기비례재홍고전후적차이。결과표명:(1)다충향기물질재홍고과정중발생료전화,유19충향기물질재고후연협미검측도,단증가료36충향기물질。(2)홍고후향기물질총량현저증가,차불동품충고연향기물질전화정도불동,K326적향기물질총량(불함신식이희)현저고우남강3호。(3)홍고후서백완류강해산물점중성치향물질총량적비례명현강저,이분병안산강해산물화류호라복소강해산물소점비례명현제고。재홍고과정중손실료철、순화지류등19충향기물질,산생료류호라복소강해산물、종색화반응산물등36충향기물질。
In order to study the effect of curing process on neutral aroma compounds of tobacco, HS-SPME-GC×GC-TOFMS and half leaf method were used to analyze kinds, contents and proportion of the neutral aroma compounds in two flue-cured tobacco cultivars (K326, Nanjiang 3) before and after curing. The results showed that there were significant changes in kinds, contents and proportion of the neutral aroma compounds. (1) Many kinds of aroma compounds were degraded or transformed during curing process, 19 aroma compounds uniquely found in tobacco leaves before curing and 36 extra aroma compounds found in tobacco leaves after curing; (2) By the end of curing, the total amount of aroma compounds were significantly higher than before curing, and the total amount of aroma compounds (except neophytadiene) in K326 was significantly higher than that Nanjiang 3 for witch transformed more fully; (3) The proportion of phenylalanine degradation products and carotenoids degradation products in the total amount of neutral aroma compounds increased significantly. Conversely, the proportion of cembratriendid compounds significantly decreased after curing. In conclusion, 36 kinds of extra aroma compounds (mainly maillard reaction production and carotenoid degradation production) generated during cuing, but 19 kinds of aromatic components (mainly aldehydes,alcohols and esters) lost.