CAJ | 학술논문

分析比较水蒸汽蒸馏法与乙醇提取化橘红叶化学成分的差异。通过水蒸汽蒸馏提取和无水乙醇超声辅助提取化橘红叶中的化学成分，运用GC-MS技术对其成分进行分离鉴定，用峰面积归一化法进行定量分析。水蒸汽蒸馏提取法共分离出58种成分，鉴定出其中的18种，主要成分是：β-蒎烯（19.44%）、β-月桂烯（6.95%）、D-柠檬烯（10.49%）、γ-萜品烯（19.30%）和石竹烯（20.46%）等；乙醇提取法共分离出80种成分，鉴定出其中的43种，主要成分是亚油酸（16.8%）、硬脂酸（6.57%）、菜油甾醇（5.82%）、豆甾烯醇（7.12%）和扶桑甾醇氧化物（14.28%）等，同时鉴定了甲氧基香豆素、补骨脂素、佛手柑内酯、前胡内酯和橙皮油内酯等香豆素类化合物，以及柚皮素、角鲨烯和VE等活性成分。两种不同的提取法共分离鉴定了18种相同的化学成分，乙醇提取法多分离鉴定25种成分。
분석비교수증기증류법여을순제취화귤홍협화학성분적차이。통과수증기증류제취화무수을순초성보조제취화귤홍협중적화학성분，운용GC-MS기술대기성분진행분리감정，용봉면적귀일화법진행정량분석。수증기증류제취법공분리출58충성분，감정출기중적18충，주요성분시：β-파희（19.44%）、β-월계희（6.95%）、D-저몽희（10.49%）、γ-첩품희（19.30%）화석죽희（20.46%）등；을순제취법공분리출80충성분，감정출기중적43충，주요성분시아유산（16.8%）、경지산（6.57%）、채유치순（5.82%）、두치희순（7.12%）화부상치순양화물（14.28%）등，동시감정료갑양기향두소、보골지소、불수감내지、전호내지화등피유내지등향두소류화합물，이급유피소、각사희화VE등활성성분。량충불동적제취법공분리감정료18충상동적화학성분，을순제취법다분리감정25충성분。
To analyse the chemical constituent of the extracts from leaves of Exocarpium Citrus Grandis by different extraction methods. The compounds were extracted by steam distillation and ethanol separately , constituents were separated and identified by GC-MS , and were quantified by the accuracy of area percent. 58 components were separated , among which 18 were identified, the main components wereβ-Pinene (19.44%),β-Myrcene (6.95%), Limonene (10.49%),γ-Terpinene (19.30%) and Caryophyllene (20.46%) by steam distillation. 80 components were separated , among which 43 were identified , the main components were fatty acids (23.27%) and sterols (27.22%), the main active ingredients were five cumarins (Herniarin, Ficusin, Bergapte, Ammidin and Aurapten), Naringenin, Supraene and Vitamin E in the alcohol extraction. 18 chemical components of the extracts were the same by the two extraction methods, but there were more than 25 components in the alcohol extraction.