中医药信息
中醫藥信息
중의약신식
INFORMATION ON TRADITIONAL CHINESE MEDICINE
2015年
4期
23-25
,共3页
潘娟%杨炳友%王欣%匡海学
潘娟%楊炳友%王訢%劻海學
반연%양병우%왕흔%광해학
茄科%过氧化麦角甾醇%大孔树脂%D941
茄科%過氧化麥角甾醇%大孔樹脂%D941
가과%과양화맥각치순%대공수지%D941
Solanaceae%Ergosterol peroxide%Macroporous resins%D941
目的:研究洋金花中甾体类化学成分。方法:采用大孔吸附树脂、硅胶等柱色谱方法进行分离和纯化,利用质谱和核磁测试技术进行化合物的结构鉴定。结果:从洋金花70%乙醇提取物中分离并鉴定了5个甾体类化合物,分别为过氧化麦角甾醇(1),Alkesterol B(2),Lucium substance B(3),β-谷甾醇(4)和豆甾醇(5)。结论:化合物1为首次从茄科中分离得到。
目的:研究洋金花中甾體類化學成分。方法:採用大孔吸附樹脂、硅膠等柱色譜方法進行分離和純化,利用質譜和覈磁測試技術進行化閤物的結構鑒定。結果:從洋金花70%乙醇提取物中分離併鑒定瞭5箇甾體類化閤物,分彆為過氧化麥角甾醇(1),Alkesterol B(2),Lucium substance B(3),β-穀甾醇(4)和豆甾醇(5)。結論:化閤物1為首次從茄科中分離得到。
목적:연구양금화중치체류화학성분。방법:채용대공흡부수지、규효등주색보방법진행분리화순화,이용질보화핵자측시기술진행화합물적결구감정。결과:종양금화70%을순제취물중분리병감정료5개치체류화합물,분별위과양화맥각치순(1),Alkesterol B(2),Lucium substance B(3),β-곡치순(4)화두치순(5)。결론:화합물1위수차종가과중분리득도。
Objective: To investigate the chemical constituents of sterides from Dautra Mete l L..Methods: A variety of column chromatographies such as macroporous resins and silica gel were used in the isolation and purification, and MS along with NMR was adopted to determine the structures.Results:Five compounds were isolated and purified from the 70%ethanol extract of Datura Metel L., Ergosterol peroxide (1), Alkesterol B (2), Lucium substance B (3), β-Sitosterol (4), Stigmasterol (5).Conclusion: Compound 1 is isolated and reported from Solanaceae for the first time.