西南师范大学学报(自然科学版)
西南師範大學學報(自然科學版)
서남사범대학학보(자연과학판)
JOURNAL OF SOUTHWEST CHINA NORMAL UNIVERSITY
2015年
6期
101-106
,共6页
廖洪波%岑丽%王若茜%朱姗姗%杨晓明
廖洪波%岑麗%王若茜%硃姍姍%楊曉明
료홍파%잠려%왕약천%주산산%양효명
纳米材料%碳点%一步合成法
納米材料%碳點%一步閤成法
납미재료%탄점%일보합성법
nanomaterials%carbon dots%one-step synthesis method
碳点作为碳纳米材料的新成员,具有良好的光学稳定性和生物低毒性,倍受人们关注。现有关制备碳点的方法层出不穷,但合成碳点的产率低且过程繁琐,消耗过大,浪费过多,不够方便快捷。研究以适当比例的组氨酸、五氧化二磷和超纯水混合,一步碳化法合成碳点的方法,其合成的碳点分散性良好,在不同的盐浓度、pH、温度下荧光信号都很稳定,荧光寿命较长,且在常温下便可进行,合成条件要求低,简便且经济,优于传统的制备方法。该碳点其优良的性能在纳米材料用于检测分析及生物成像方面具有潜在的意义。
碳點作為碳納米材料的新成員,具有良好的光學穩定性和生物低毒性,倍受人們關註。現有關製備碳點的方法層齣不窮,但閤成碳點的產率低且過程繁瑣,消耗過大,浪費過多,不夠方便快捷。研究以適噹比例的組氨痠、五氧化二燐和超純水混閤,一步碳化法閤成碳點的方法,其閤成的碳點分散性良好,在不同的鹽濃度、pH、溫度下熒光信號都很穩定,熒光壽命較長,且在常溫下便可進行,閤成條件要求低,簡便且經濟,優于傳統的製備方法。該碳點其優良的性能在納米材料用于檢測分析及生物成像方麵具有潛在的意義。
탄점작위탄납미재료적신성원,구유량호적광학은정성화생물저독성,배수인문관주。현유관제비탄점적방법층출불궁,단합성탄점적산솔저차과정번쇄,소모과대,낭비과다,불구방편쾌첩。연구이괄당비례적조안산、오양화이린화초순수혼합,일보탄화법합성탄점적방법,기합성적탄점분산성량호,재불동적염농도、pH、온도하형광신호도흔은정,형광수명교장,차재상온하편가진행,합성조건요구저,간편차경제,우우전통적제비방법。해탄점기우량적성능재납미재료용우검측분석급생물성상방면구유잠재적의의。
Carbon dots have attracted much attention as a new member of carbon nanomaterials owing to the excellent optical stability and low biotoxicity .Nowadays methods for the preparation of carbon dots are emerging one after another with the shortages of low yield ,complicated process ,consuming too much and inconvenience .It is supposed to put forward a simple synthesis method .In this study ,carbon dots have been synthesized by means of a one‐step synthesis method with an appropriate proportion of histidine , phosphorus pentoxide and ultra‐pure water mixed directly .The carbon dots synthesized by this method show satisfactory dispersity ,long fluorescence lifetime and stable fluorescence intensity in the environment of different salinity ,power of hydrogen (pH) ,temperature and time stability test factors .It can react at room temperature which requires less conditions factor ,cost less and can be simpler than others .As to the traditional synthesis method ,this carbon dots have potential meaning in detection analysis and biological imaging due to its excellent performance for application in nanomaterials .