天津工业大学学报
天津工業大學學報
천진공업대학학보
JOURNAL OF TIANJIN POLYTECHNIC UNIVERSITY
2015年
3期
16-19,23
,共5页
王春红%贾瑞婷%何顺辉%徐磊%郑振荣
王春紅%賈瑞婷%何順輝%徐磊%鄭振榮
왕춘홍%가서정%하순휘%서뢰%정진영
洋麻纤维%碱氧-浴%精细化处理%多指标正交分析%表面粗糙度%可纺性
洋痳纖維%堿氧-浴%精細化處理%多指標正交分析%錶麵粗糙度%可紡性
양마섬유%감양-욕%정세화처리%다지표정교분석%표면조조도%가방성
kenaf fibers%alkali and hydrogen peroxide%fine treatment%multiple indicator orthogonal analysis%surface roughness%spinnability
为了提高洋麻纤维的可纺性,采用碱氧-浴一步柔软方法对洋麻进行精细化处理.利用多指标正交实验方法对总碱浓度、先加入碱浓度、双氧水浓度及碱煮时间这4个参数进行工艺优化设计,通过对纤维细度、断裂强度、柔软度3个指标的综合分析评定最佳处理工艺,并对处理后的洋麻纤维进行基本性能及扫描电子显微镜、傅里叶红外光谱测试.结果表明:最佳处理工艺是总碱质量分数为10%、先加入的碱质量分数为1.2%、双氧水质量分数为1.2%、处理时间为2.5 h;精细化处理的洋麻纤维细度、柔软度、断裂强度分别为13.83 dtex、33.75 r/10 cm、4.13 cN/dtex,与未处理纤维相比,分别降低66.1%、提高25.1%、提高25.9%;扫描电子显微镜及傅里叶红外光谱表明纤维杂质减少,表面粗糙度增加,可纺性提高.
為瞭提高洋痳纖維的可紡性,採用堿氧-浴一步柔軟方法對洋痳進行精細化處理.利用多指標正交實驗方法對總堿濃度、先加入堿濃度、雙氧水濃度及堿煮時間這4箇參數進行工藝優化設計,通過對纖維細度、斷裂彊度、柔軟度3箇指標的綜閤分析評定最佳處理工藝,併對處理後的洋痳纖維進行基本性能及掃描電子顯微鏡、傅裏葉紅外光譜測試.結果錶明:最佳處理工藝是總堿質量分數為10%、先加入的堿質量分數為1.2%、雙氧水質量分數為1.2%、處理時間為2.5 h;精細化處理的洋痳纖維細度、柔軟度、斷裂彊度分彆為13.83 dtex、33.75 r/10 cm、4.13 cN/dtex,與未處理纖維相比,分彆降低66.1%、提高25.1%、提高25.9%;掃描電子顯微鏡及傅裏葉紅外光譜錶明纖維雜質減少,錶麵粗糙度增加,可紡性提高.
위료제고양마섬유적가방성,채용감양-욕일보유연방법대양마진행정세화처리.이용다지표정교실험방법대총감농도、선가입감농도、쌍양수농도급감자시간저4개삼수진행공예우화설계,통과대섬유세도、단렬강도、유연도3개지표적종합분석평정최가처리공예,병대처리후적양마섬유진행기본성능급소묘전자현미경、부리협홍외광보측시.결과표명:최가처리공예시총감질량분수위10%、선가입적감질량분수위1.2%、쌍양수질량분수위1.2%、처리시간위2.5 h;정세화처리적양마섬유세도、유연도、단렬강도분별위13.83 dtex、33.75 r/10 cm、4.13 cN/dtex,여미처리섬유상비,분별강저66.1%、제고25.1%、제고25.9%;소묘전자현미경급부리협홍외광보표명섬유잡질감소,표면조조도증가,가방성제고.
In order to improve the spinnability of the kenaf fibres, alkali oxygen-soft bath step method was used in refinement process for kenaf. Four parameters, such as alkali treatment time, concentrations of pre-alkalithe, alkali and hydrogen peroxide were optimized by multiple indicator orthogonal experimental method based on the evaluation factors of fiber fineness, breaking strength and softness. The basic physical properties, SEM, FTIR of treated kenaf fiber were tested. The results showed that the optimal parameters were alkali concentration of 10%, pre-alkalithe concentration of 1.2%, hydrogen peroxide concentration of 1.2%, and treatment time of 2.5 h. The refinement fineness, softness, and breaking strength of Kenaf fiber are 13.83 dtex, 33.75 r/10 cm, 4.13 cN/dtex respectively, compared with those of untreated fibers, that reduced by 66.1%, improved by 25.1%, improved by 25.9%!respectively. SEM and FTIR show that the fine treatment fibers have low surface impurities, high surface roughness and soimproved spinnability.