安徽大学学报(自然科学版)
安徽大學學報(自然科學版)
안휘대학학보(자연과학판)
JOURNAL OF ANHUI UNIVERSITY(NATURAL SCIENCES EDITION)
2015年
4期
72-78
,共7页
袁海%胡俊杰%张恩贡%李鹏%袁孝友
袁海%鬍俊傑%張恩貢%李鵬%袁孝友
원해%호준걸%장은공%리붕%원효우
Au-ZnO纳米颗粒%六棱柱%光催化
Au-ZnO納米顆粒%六稜柱%光催化
Au-ZnO납미과립%륙릉주%광최화
Au-ZnO nanocomposite%hexagonal prism%photocatalytic property
采用一步法制备结构均一的六棱柱状Au‐ZnO复合纳米材料,并通过X射线衍射仪(XRD)、扫描电子显微镜(SEM )等对其结构和形貌进行表征.结果表明,改变 HAuCl4的用量能够很好地调控所合成的纳米复合物的形貌.在此基础上,研究了Au‐ZnO纳米颗粒的光催化性能,当Au含量为2.65%时,所合成纳米复合物对罗丹明B染料的光降解能力最佳,降解率达到99.6%.
採用一步法製備結構均一的六稜柱狀Au‐ZnO複閤納米材料,併通過X射線衍射儀(XRD)、掃描電子顯微鏡(SEM )等對其結構和形貌進行錶徵.結果錶明,改變 HAuCl4的用量能夠很好地調控所閤成的納米複閤物的形貌.在此基礎上,研究瞭Au‐ZnO納米顆粒的光催化性能,噹Au含量為2.65%時,所閤成納米複閤物對囉丹明B染料的光降解能力最佳,降解率達到99.6%.
채용일보법제비결구균일적륙릉주상Au‐ZnO복합납미재료,병통과X사선연사의(XRD)、소묘전자현미경(SEM )등대기결구화형모진행표정.결과표명,개변 HAuCl4적용량능구흔호지조공소합성적납미복합물적형모.재차기출상,연구료Au‐ZnO납미과립적광최화성능,당Au함량위2.65%시,소합성납미복합물대라단명B염료적광강해능력최가,강해솔체도99.6%.
In this paper ,uniform hexagonal prism Au‐ZnO nanocomposite was successfully synthesized by one‐step reaction .The structure and morphology of Au‐ZnO nanocomposite were characterized using XRD , TEM , SEM , respectively . The results show that the morphology of Au‐ZnO could be controlled by changing the amount of HAuCl4 . On the basis ,the photocatalytic performance of the Au‐ZnO nanocomposite was investigated .When the content of the Au was 2.65% ,the efficiency of photocatalytic degraded rhodamine B was the best ,and the degradation rate could reach 99.6% .