中国现代中药
中國現代中藥
중국현대중약
MODERN CHINESE MEDICINE
2015年
7期
718-721
,共4页
曾恕芬%陈金东%任杨帆%陈荣洁
曾恕芬%陳金東%任楊帆%陳榮潔
증서분%진금동%임양범%진영길
熟三七配方颗粒%高效液相色谱%薄层色谱法
熟三七配方顆粒%高效液相色譜%薄層色譜法
숙삼칠배방과립%고효액상색보%박층색보법
Steamed Notoginseng formula granules%HPLC%TLC
目的：进行熟三七配方颗粒的质量标准研究，建立质量评价方法，为科学评价其质量提供依据。方法：采用薄层色谱法（TLC）对熟三七配方颗粒中人参皂苷 Rh1、Rg3进行鉴别，采用高效液相色谱法（HPLC）对其三七皂苷 R1，人参皂苷 Rg1、Re、Rb1、Rd 进行含量检测分析。结果：建立了熟三七配方颗粒中人参皂苷 Rh1、Rg3的薄层鉴别方法；建立了检测熟三七配方颗粒中三七皂苷 R1，人参皂苷 Rg1、Re、Rb1、Rd 的含量测定方法。结论：该方法简单、准确、专属性好，能有效对熟三七配方颗粒的质量进行评价。
目的：進行熟三七配方顆粒的質量標準研究，建立質量評價方法，為科學評價其質量提供依據。方法：採用薄層色譜法（TLC）對熟三七配方顆粒中人參皂苷 Rh1、Rg3進行鑒彆，採用高效液相色譜法（HPLC）對其三七皂苷 R1，人參皂苷 Rg1、Re、Rb1、Rd 進行含量檢測分析。結果：建立瞭熟三七配方顆粒中人參皂苷 Rh1、Rg3的薄層鑒彆方法；建立瞭檢測熟三七配方顆粒中三七皂苷 R1，人參皂苷 Rg1、Re、Rb1、Rd 的含量測定方法。結論：該方法簡單、準確、專屬性好，能有效對熟三七配方顆粒的質量進行評價。
목적：진행숙삼칠배방과립적질량표준연구，건립질량평개방법，위과학평개기질량제공의거。방법：채용박층색보법（TLC）대숙삼칠배방과립중인삼조감 Rh1、Rg3진행감별，채용고효액상색보법（HPLC）대기삼칠조감 R1，인삼조감 Rg1、Re、Rb1、Rd 진행함량검측분석。결과：건립료숙삼칠배방과립중인삼조감 Rh1、Rg3적박층감별방법；건립료검측숙삼칠배방과립중삼칠조감 R1，인삼조감 Rg1、Re、Rb1、Rd 적함량측정방법。결론：해방법간단、준학、전속성호，능유효대숙삼칠배방과립적질량진행평개。
Objective:To establish the quality standard for steamed Notoginseng formula granules,and provide a basis for scientific evaluation of its quality.Methods:Ginsenosides Rh1 and ginsenoside Rg3 in steamed Notoginseng formula granules were identified by TLC,and the contents of notoginsenoside R1 ,ginsenosides Rg1,Re,Rb1 ,Rd in steamed Notoginseng formula granules were determined by HPLC.Results:To established a method to identify Panax ginseng saponin Rh1 and ginsenoside Rg3 in Steamed Notoginseng Formula Granules by TLC;to establish a method to detect the content of Panax notoginsenoside R1 ,ginsenosides Rg1 ,Re,Rb1 ,Rd in Steamed Formula Notoginseng Granules.Conclusion:The established method is simple,accurate,reproducible,and it can be used as a quality control method for steamed Notoginseng formula granules.
