CAJ | 학술논문

介绍了在低温水浴中采用溶剂蒸发法合成硼酸盐晶体[C6N4H20]0．5[B5O6（OH）4]的实验。分别采用X射线粉末衍射仪、热重分析仪和红外分析仪对样品进行了表征，通过对不同大型仪器的使用，能够使学生掌握仪器操作的方法、提高谱图解析的能力。该实验为最新的科学研究成果，知识点新颖，同时将无机合成实验与大型仪器表征有机的结合在一起，不仅能够提高学生的科研能力，还能培养学生的创新思维。
개소료재저온수욕중채용용제증발법합성붕산염정체[C6N4H20]0．5[B5O6（OH）4]적실험。분별채용X사선분말연사의、열중분석의화홍외분석의대양품진행료표정，통과대불동대형의기적사용，능구사학생장악의기조작적방법、제고보도해석적능력。해실험위최신적과학연구성과，지식점신영，동시장무궤합성실험여대형의기표정유궤적결합재일기，불부능구제고학생적과연능력，환능배양학생적창신사유。
A compound [C6N4H20]0.5[B5O6(OH)4] which was synthesized by the solvent evaporation method using water as solvent at low temperature was introduced.The product was characterized by X-ray diffraction, thermogravimetry analysis and infrared spectroscopy.The students could master the instrument operation and the ability of spectrum analysis would be improved.This experiment is a latest scientific research result and has a novel knowledge.It can combine the inorganic synthesis experiment and large-scale instruments. The ability of scientific research of students could be improved and the innovative thinking would be developed.