广州化工
廣州化工
엄주화공
GUANGZHOU CHEMICAL INDUSTRY AND TECHNOLOGY
2015年
15期
89-90,121
,共3页
刘少峰%许磊%张敬宝%范家辉
劉少峰%許磊%張敬寶%範傢輝
류소봉%허뢰%장경보%범가휘
钛酸盐纳米管%溶剂热法%酯化反应
鈦痠鹽納米管%溶劑熱法%酯化反應
태산염납미관%용제열법%지화반응
titanate nanotubes%solvothermal method%esterification reaction
H2 Ti2 O5纳米管用溶剂热方法制备,将其应用于酸催化酯化反应。通过X-射线粉末衍射、 NH3程序升温脱附对H2 Ti2 O5纳米管进行表征,结果表明,所制备的H2 Ti2 O5纳米管有两种强度的酸中心,即弱酸中心和中等强度的酸中心,以H2 Ti2 O5纳米管为催化剂,乙酸和正丁醇的酯化反应效率可达到45.57%。
H2 Ti2 O5納米管用溶劑熱方法製備,將其應用于痠催化酯化反應。通過X-射線粉末衍射、 NH3程序升溫脫附對H2 Ti2 O5納米管進行錶徵,結果錶明,所製備的H2 Ti2 O5納米管有兩種彊度的痠中心,即弱痠中心和中等彊度的痠中心,以H2 Ti2 O5納米管為催化劑,乙痠和正丁醇的酯化反應效率可達到45.57%。
H2 Ti2 O5납미관용용제열방법제비,장기응용우산최화지화반응。통과X-사선분말연사、 NH3정서승온탈부대H2 Ti2 O5납미관진행표정,결과표명,소제비적H2 Ti2 O5납미관유량충강도적산중심,즉약산중심화중등강도적산중심,이H2 Ti2 O5납미관위최화제,을산화정정순적지화반응효솔가체도45.57%。
H2 Ti2 O5 nanotubes were synthesized by solvothermal method and applied in the acid catalytic esterification reaction.The as-prepared sample was characterized by means of X-ray powder diffraction and NH3-temperature programmed desorption.The results revealed that they have two acid sites, attributing to the weak and moderate-intensity acid sites.The esterification efficiency of acetic acid and n-butanol over H2 Ti2 O5 naotubes catalyst reached to 45.57%.