广州化工
廣州化工
엄주화공
GUANGZHOU CHEMICAL INDUSTRY AND TECHNOLOGY
2015年
14期
88-90
,共3页
木薯淀粉%羟丙基乙酰化双淀粉己二酸酯%凝沉性%冻融稳定性
木藷澱粉%羥丙基乙酰化雙澱粉己二痠酯%凝沉性%凍融穩定性
목서정분%간병기을선화쌍정분기이산지%응침성%동융은정성
cassava starch%acetylated distarch adipate%retrogradation%freeze-thaw stability
采用已二酸与乙酸酐对木薯淀粉进行改性制备乙酰化双淀粉己二酸酯,得出最佳工艺条件为:淀粉乳初始浓度30%, pH 8,反应时间90 min,混合酸酐加入量4.5%,羟丙基取代度为0.1264,酯化取代度为0.031。考察了羟丙基乙酰化双淀粉己二酸酯的凝沉性、冻融稳定性和透明度,其中抗凝沉性和冻融稳定性都有了很大的提高,溶解度和透明度略微降低。
採用已二痠與乙痠酐對木藷澱粉進行改性製備乙酰化雙澱粉己二痠酯,得齣最佳工藝條件為:澱粉乳初始濃度30%, pH 8,反應時間90 min,混閤痠酐加入量4.5%,羥丙基取代度為0.1264,酯化取代度為0.031。攷察瞭羥丙基乙酰化雙澱粉己二痠酯的凝沉性、凍融穩定性和透明度,其中抗凝沉性和凍融穩定性都有瞭很大的提高,溶解度和透明度略微降低。
채용이이산여을산항대목서정분진행개성제비을선화쌍정분기이산지,득출최가공예조건위:정분유초시농도30%, pH 8,반응시간90 min,혼합산항가입량4.5%,간병기취대도위0.1264,지화취대도위0.031。고찰료간병기을선화쌍정분기이산지적응침성、동융은정성화투명도,기중항응침성화동융은정성도유료흔대적제고,용해도화투명도략미강저。
Acetylated distarch adipates was prepared by cassava starch with adipic acetic mixed anhydride.It showed that the optimal parameters were initial starch slurry concentration 30%, pH 8, reaction time 1.5 h and mixed anhydride concentration 4.5%, respectively. The degree of hydroxypropyl substitution was 0.1264 , mixed anhydride molar substitution degree was 0.031.The properties of retrogradation, freeze-thaw stability and the degree of clarity were studied, retrogradation and freeze-thaw stability of acetylated distarch adipates had been greatly improved, and solubility and transparency were slightly lower than cassava starch.