CAJ | 학술논문

目的：研究并优化大孔吸附树脂分离纯化闽产钩吻根中总生物碱。方法先以总生物碱含量为考察指标，从3种不同型号的树脂中筛选出分离纯化闽产钩吻根总生物碱的最佳树脂，再对最佳树脂吸附工艺参数进行全面优化。结果 AB－8型大孔吸附树脂对闽产钩吻根总生物碱的吸附与解析性能较好，确定最佳洗脱条件为90％乙醇洗脱，溶剂用量4BV。结论 AB－8型大孔吸附树脂可有效地分离纯化闽产钩吻根总生物碱。
목적：연구병우화대공흡부수지분리순화민산구문근중총생물감。방법선이총생물감함량위고찰지표，종3충불동형호적수지중사선출분리순화민산구문근총생물감적최가수지，재대최가수지흡부공예삼수진행전면우화。결과 AB－8형대공흡부수지대민산구문근총생물감적흡부여해석성능교호，학정최가세탈조건위90％을순세탈，용제용량4BV。결론 AB－8형대공흡부수지가유효지분리순화민산구문근총생물감。
OBJECTIVE To optimize the separation and purification of total alkaloids from Gelsemium elegans Benth.Root of Fujian by macroporous resin .METHODS Three types of macroporous resins were used to separate and purify alkaloids.Contents of the total alkaloids were compared in order to find the optimum macroporous resin ,and its technical process was comprehensive optimized .RESULTS AB-8 was selected for its excellent adsorptionand desorption properties.The best elution solution technical process was 4BV of 90% ethanol.CONCLUSION The total alkaloids of Gelsemium elegans Benth.Root of Fujian can be effectively separated and purificated by AB -8macroporous resin.