分析仪器
分析儀器
분석의기
ANALYTICAL INSTRUMENTATION
2015年
4期
50-52
,共3页
向元斌%胡强%李蓓佳%黄本芬%吴蔚%吕晓艇
嚮元斌%鬍彊%李蓓佳%黃本芬%吳蔚%呂曉艇
향원빈%호강%리배가%황본분%오위%려효정
电感耦合等离子体发射光谱法%聚氯化铝%三氧化二铝
電感耦閤等離子體髮射光譜法%聚氯化鋁%三氧化二鋁
전감우합등리자체발사광보법%취록화려%삼양화이려
inductively coupled plasma atomic emission spectrometry%poly aluminum chloride%alumi-num oxide
建立了用电感耦合等离子发射光谱法(ICP‐OES)测定聚氯化铝中的三氧化二铝的方法。分析谱线为Al309.217 nm ,铝的浓度在0.009 mg/L~100 mg/L范围内时,校准曲线的线性相关系数R大于0.9999,检出限为0.009mg/L ,方法的加标回收率在98%~102%之间,用该法对不同含量的聚氯化铝样品进行分析,测定结果与国标法测定结果基本相符。本方法简便、快速,适合聚氯化铝中三氧化二铝的测定。
建立瞭用電感耦閤等離子髮射光譜法(ICP‐OES)測定聚氯化鋁中的三氧化二鋁的方法。分析譜線為Al309.217 nm ,鋁的濃度在0.009 mg/L~100 mg/L範圍內時,校準麯線的線性相關繫數R大于0.9999,檢齣限為0.009mg/L ,方法的加標迴收率在98%~102%之間,用該法對不同含量的聚氯化鋁樣品進行分析,測定結果與國標法測定結果基本相符。本方法簡便、快速,適閤聚氯化鋁中三氧化二鋁的測定。
건립료용전감우합등리자발사광보법(ICP‐OES)측정취록화려중적삼양화이려적방법。분석보선위Al309.217 nm ,려적농도재0.009 mg/L~100 mg/L범위내시,교준곡선적선성상관계수R대우0.9999,검출한위0.009mg/L ,방법적가표회수솔재98%~102%지간,용해법대불동함량적취록화려양품진행분석,측정결과여국표법측정결과기본상부。본방법간편、쾌속,괄합취록화려중삼양화이려적측정。
A method for determination of aluminum oxide in poly aluminum chloride by inductively coupled plasma atomic emission spectrometry (ICP‐OES) was established. The analysitical line of Al was 309. 217nm .When the concentration of aluminum w as in the range of 0. 009 mg /L 100 mg /L ,the line‐ar correlation coefficient R of calibration curve was more than 0.9999 ,the detection limit was 0.009mg/L , the standard addition recoveries ranged from 98% to 102% .Poly aluminum chloride samples with differ‐ent contents were analyzed ,the results were basically consistent with national standard method. The meth‐od is simple ,fast and suitable for the determination of aluminum oxide in poly aluminum chloride .