国际中医中药杂志
國際中醫中藥雜誌
국제중의중약잡지
INTERNATIONAL JOURNAL OF TRIDITIONAL CHINESE MEDICINE
2015年
8期
728-730
,共3页
刘辉%邓莉%王盟%赵亚鑫%张爱兰
劉輝%鄧莉%王盟%趙亞鑫%張愛蘭
류휘%산리%왕맹%조아흠%장애란
牙疼舒滴丸%正交试验%欧前胡素%高效液相色谱
牙疼舒滴汍%正交試驗%歐前鬍素%高效液相色譜
아동서적환%정교시험%구전호소%고효액상색보
Toothache drop pills%Orthogonal test%Imperatorin%High-performance liquidchromatography
目的：制备牙疼舒滴丸并建立其质量标准。方法采用滴制法制备牙疼舒滴丸，采用高效液相色谱法测定本制剂中欧前胡素含量。结果制得的滴丸大小均匀、圆整光滑、硬度适中；薄层色谱法可鉴别出欧前胡素的特征斑点；欧前胡素在0.50～520μg/ml范围内线性关系良好，r＝0.9998，平均加样回收率范围为98.38%，RSD值为1.05%。结论该制备方法简单，滴丸成形性好，质量可控。
目的：製備牙疼舒滴汍併建立其質量標準。方法採用滴製法製備牙疼舒滴汍，採用高效液相色譜法測定本製劑中歐前鬍素含量。結果製得的滴汍大小均勻、圓整光滑、硬度適中；薄層色譜法可鑒彆齣歐前鬍素的特徵斑點；歐前鬍素在0.50～520μg/ml範圍內線性關繫良好，r＝0.9998，平均加樣迴收率範圍為98.38%，RSD值為1.05%。結論該製備方法簡單，滴汍成形性好，質量可控。
목적：제비아동서적환병건립기질량표준。방법채용적제법제비아동서적환，채용고효액상색보법측정본제제중구전호소함량。결과제득적적환대소균균、원정광활、경도괄중；박층색보법가감별출구전호소적특정반점；구전호소재0.50～520μg/ml범위내선성관계량호，r＝0.9998，평균가양회수솔범위위98.38%，RSD치위1.05%。결론해제비방법간단，적환성형성호，질량가공。
Objective To prepare toothache drop pills and establish its quality standard.Methods The drop pills were prepared by a routine method; HPLC was used for the determination of the EU isoimperatorin content.Results The drop pills were well- distributed in size, smooth and glossy in appearance, mild in hardness; TLC can identify isoimperatorin characteristic spots; Determination of the Indigo 0.50~520μg/ml linear relationship was good,r=0.999 8, the recovery of 98.38%.RSD values were 1.05%.Conclusion The preparation method of toothache drop pills is simple, and the drop pills are well-shaped with controllable quality.
