中国药师
中國藥師
중국약사
CHINA PHARMACIST
2015年
8期
1404-1406
,共3页
肉苁蓉%松果菊苷%毛蕊花糖苷%一测多评法%高效液相色谱法
肉蓯蓉%鬆果菊苷%毛蕊花糖苷%一測多評法%高效液相色譜法
육종용%송과국감%모예화당감%일측다평법%고효액상색보법
Cistanche%Echinacoside%Acteoside%Quantitative analysis of multi-components by single marker%HPLC
目的：：建立同时测定肉苁蓉中松果菊苷、毛蕊花糖苷的高效液相色谱一测多评法。方法：以松果菊苷和毛蕊花糖苷为考察指标，建立两者间的相对校正因子，并用校正因子计算另一个成分的含量，将一测多评法的计算值与外标法实测值进行比较。结果：建立的相对校正因子重现性良好，采用校正因子计算的含量值和外标法实测值之间没有显著性差异。结论：同时测定肉苁蓉中2种成分的一测多评法方法可靠，结果准确，可用于控制肉苁蓉药材及其饮片的质量。
目的：：建立同時測定肉蓯蓉中鬆果菊苷、毛蕊花糖苷的高效液相色譜一測多評法。方法：以鬆果菊苷和毛蕊花糖苷為攷察指標，建立兩者間的相對校正因子，併用校正因子計算另一箇成分的含量，將一測多評法的計算值與外標法實測值進行比較。結果：建立的相對校正因子重現性良好，採用校正因子計算的含量值和外標法實測值之間沒有顯著性差異。結論：同時測定肉蓯蓉中2種成分的一測多評法方法可靠，結果準確，可用于控製肉蓯蓉藥材及其飲片的質量。
목적：：건립동시측정육종용중송과국감、모예화당감적고효액상색보일측다평법。방법：이송과국감화모예화당감위고찰지표，건립량자간적상대교정인자，병용교정인자계산령일개성분적함량，장일측다평법적계산치여외표법실측치진행비교。결과：건립적상대교정인자중현성량호，채용교정인자계산적함량치화외표법실측치지간몰유현저성차이。결론：동시측정육종용중2충성분적일측다평법방법가고，결과준학，가용우공제육종용약재급기음편적질량。
To establish a determination method for two effective components echinacoside and acteoside in cistanche by quantitative analysis of multi-components by single marker ( QAMS) . Methods:With echinacea glycosides and mullein indican as the examining indices, the relative correction factor ( RCF) between echinacea glycosides and mullein indican was established, and then used to calculate the content of the other components. Meanwhile, the calculated value was compared with that of the external standard method. Results:The RCFs had good reproducibility without significant differences between the quantitative results of QAMS method and those of the external standard method. Conclusion:The described method is reliable and accurate, and can be used to control the quality of echinacoside and acteoside in cistanche.
