实用药物与临床
實用藥物與臨床
실용약물여림상
PRACTICAL PHARMACY AND CLINICAL REMEDIES
2015年
8期
957-958
,共2页
段立爽%单会娇%齐歆%杨文
段立爽%單會嬌%齊歆%楊文
단립상%단회교%제흠%양문
黄柏%关黄柏%混用%薄层色谱
黃柏%關黃柏%混用%薄層色譜
황백%관황백%혼용%박층색보
Phellodendri chinensis cortex%Phellodendri amurensis cortex%Mixing%TLC
目的:分析成方制剂中黄柏、关黄柏的混用现象。方法以黄柏、关黄柏、盐酸巴马汀、盐酸小檗碱为对照,与3批妇炎康片样品溶液点于同一块薄层板上,分别在两种不同的展开剂中展开,展开后,晾干,于365 nm紫外光下检视。结果在与盐酸巴马汀、盐酸小檗碱、黄柏、关黄柏相应的位置上均呈现相同颜色的荧光斑点。结论采用两种展开系统同时进行展开,试验结果一致,验证了该品种的成方制剂中使用了关黄柏替代黄柏入药或二者同时入药的可能性。
目的:分析成方製劑中黃柏、關黃柏的混用現象。方法以黃柏、關黃柏、鹽痠巴馬汀、鹽痠小檗堿為對照,與3批婦炎康片樣品溶液點于同一塊薄層闆上,分彆在兩種不同的展開劑中展開,展開後,晾榦,于365 nm紫外光下檢視。結果在與鹽痠巴馬汀、鹽痠小檗堿、黃柏、關黃柏相應的位置上均呈現相同顏色的熒光斑點。結論採用兩種展開繫統同時進行展開,試驗結果一緻,驗證瞭該品種的成方製劑中使用瞭關黃柏替代黃柏入藥或二者同時入藥的可能性。
목적:분석성방제제중황백、관황백적혼용현상。방법이황백、관황백、염산파마정、염산소벽감위대조,여3비부염강편양품용액점우동일괴박층판상,분별재량충불동적전개제중전개,전개후,량간,우365 nm자외광하검시。결과재여염산파마정、염산소벽감、황백、관황백상응적위치상균정현상동안색적형광반점。결론채용량충전개계통동시진행전개,시험결과일치,험증료해품충적성방제제중사용료관황백체대황백입약혹이자동시입약적가능성。
Objective To analyze the mixing phenomenon of Phellodendri chinensis cortex and Phellodendri amurensis cortex in fuyankang tablets. Methods The standard solutions ( phellodendri chinensis cortex,Phellodendri amurensis cortex,palmatine hydrochloride,berberine hydrochloride) and the sample solution ( three batches of fuyan-kang tablets) were pointed on the same piece of thin plate. It was expanded in two different developing agents respec-tively and observed under the view of UV light 365 nm after dried. Results In the corresponding position of the stand-ard solution,the sample solution showed fluorescent spots of the same color. Conclusion The results of the two ex-panded system were consistent. It was verified the possibility that either Phellodendri amurensis cortex was substitude for Phellodendri chinensis cortex or both the two drugs were used in the preparation of fuyankang tablets.