电子元件与材料
電子元件與材料
전자원건여재료
ELECTRONIC COMPONENTS & MATERIALS
2015年
9期
46-49
,共4页
董丽荣%宋健%于万秋%华中
董麗榮%宋健%于萬鞦%華中
동려영%송건%우만추%화중
单辊快淬法%Fe74CoxY6-xB20%非晶合金%热稳定性%晶化激活能%磁性能
單輥快淬法%Fe74CoxY6-xB20%非晶閤金%熱穩定性%晶化激活能%磁性能
단곤쾌쉬법%Fe74CoxY6-xB20%비정합금%열은정성%정화격활능%자성능
melt-spinning technique%Fe74CoxY6-xB20%amorphous alloys%thermal stability%crystallization activation energy%magnetic property
采用单辊快淬法制备合金薄带Fe74CoxY6-xB20(粒子数分数x=2,3,4)合金系,取不同的温度对合金进行热处理,用X射线衍射(XRD),差热分析仪(DSC),振动样品磁强计(VSM)等测试手段对样品的晶化过程、热性能和磁性能进行研究。结果表明:制备的Fe74CoxY6–xB20均为非晶合金,Fe74CoxY6-xB20(x=2,3,4)非晶合金的晶化激活能分别为473.7,583.0和570.1 kJ/mol,Fe74Co3Y3B20非晶合金热稳定性最好。非晶合金Fe74CoxY6-xB20(x=2,3,4)的饱和磁化强度MS分别为110,105和109 A·m2·kg–1,矫顽力都较低,适量地添加Co提高了合金的非晶形成能力和磁性能。
採用單輥快淬法製備閤金薄帶Fe74CoxY6-xB20(粒子數分數x=2,3,4)閤金繫,取不同的溫度對閤金進行熱處理,用X射線衍射(XRD),差熱分析儀(DSC),振動樣品磁彊計(VSM)等測試手段對樣品的晶化過程、熱性能和磁性能進行研究。結果錶明:製備的Fe74CoxY6–xB20均為非晶閤金,Fe74CoxY6-xB20(x=2,3,4)非晶閤金的晶化激活能分彆為473.7,583.0和570.1 kJ/mol,Fe74Co3Y3B20非晶閤金熱穩定性最好。非晶閤金Fe74CoxY6-xB20(x=2,3,4)的飽和磁化彊度MS分彆為110,105和109 A·m2·kg–1,矯頑力都較低,適量地添加Co提高瞭閤金的非晶形成能力和磁性能。
채용단곤쾌쉬법제비합금박대Fe74CoxY6-xB20(입자수분수x=2,3,4)합금계,취불동적온도대합금진행열처리,용X사선연사(XRD),차열분석의(DSC),진동양품자강계(VSM)등측시수단대양품적정화과정、열성능화자성능진행연구。결과표명:제비적Fe74CoxY6–xB20균위비정합금,Fe74CoxY6-xB20(x=2,3,4)비정합금적정화격활능분별위473.7,583.0화570.1 kJ/mol,Fe74Co3Y3B20비정합금열은정성최호。비정합금Fe74CoxY6-xB20(x=2,3,4)적포화자화강도MS분별위110,105화109 A·m2·kg–1,교완력도교저,괄량지첨가Co제고료합금적비정형성능력화자성능。
Amorphous alloys Fe74CoxY6–xB20 (x=2, 3, 4) were prepared by melt-spinning technique. Alloys were annealed at different temperatures. The thermal stability,crystalline process and magnetic property of amorphous alloys were studied by scanning calorimeter (DSC), X-ray diffraction (XRD) and vibrating sample magnetometer (VSM). The results show that all of samples are amorphous alloy. The crystallization activation energy of Fe74CoxY6–xB20 (x=2, 3, 4) are 473.7, 583.0 and 570.1 kJ/mol. Among all the amorphous alloys, Fe 74 Co 3 Y 3 B 20 has the best thermal stability. The saturation magnetizations(MS)of Fe74CoxY6–xB20 (x=2, 3, 4) are 110,105 and 109 A·m2·kg–1, respectively. The coercivity of samples are very small. Suitable addition of Co can enhance the glass forming ability and magnetic property of the alloys.