华南理工大学学报(自然科学版)
華南理工大學學報(自然科學版)
화남리공대학학보(자연과학판)
JOURNAL OF SOUTH CHINA UNIVERSITY OF TECHNOLOGY(NATURAL SCIENCE EDITION)
2015年
6期
30-36
,共7页
双离子液体%微乳液%乙二胺%酶解%桉木
雙離子液體%微乳液%乙二胺%酶解%桉木
쌍리자액체%미유액%을이알%매해%안목
double ionic liquid%microemulsion%quadrol%enzymatic hydrolysis%eucalyptus
研究了碱强化的离子液体微乳液( DILMS )体系的配比、浸渍方式及处理条件对速生阔叶材桉木酶解效率的影响,探讨了浸渍处理后原料残渣和浸渍液中单糖含量的变化,并利用离子色谱法对单位质量底物的葡萄糖增加比进行定量分析.实验结果表明:适宜的DILMS浸渍工艺参数为100℃、8 h、底物目数40(即直径180~380μm),进一步结合碱强化的乙二胺浸渍工序(70℃,3 h)而形成的“两步法”预浸渍可以使单位质量底物中葡萄糖占总还原糖的百分比由64.33%上升到96.34%,酶解得率由35.8%上升到83.2%,葡萄糖实际产量提高了1.11倍.研究表明碱强化的离子液体微乳液具有优良的预浸渍处理效果.
研究瞭堿彊化的離子液體微乳液( DILMS )體繫的配比、浸漬方式及處理條件對速生闊葉材桉木酶解效率的影響,探討瞭浸漬處理後原料殘渣和浸漬液中單糖含量的變化,併利用離子色譜法對單位質量底物的葡萄糖增加比進行定量分析.實驗結果錶明:適宜的DILMS浸漬工藝參數為100℃、8 h、底物目數40(即直徑180~380μm),進一步結閤堿彊化的乙二胺浸漬工序(70℃,3 h)而形成的“兩步法”預浸漬可以使單位質量底物中葡萄糖佔總還原糖的百分比由64.33%上升到96.34%,酶解得率由35.8%上升到83.2%,葡萄糖實際產量提高瞭1.11倍.研究錶明堿彊化的離子液體微乳液具有優良的預浸漬處理效果.
연구료감강화적리자액체미유액( DILMS )체계적배비、침지방식급처리조건대속생활협재안목매해효솔적영향,탐토료침지처리후원료잔사화침지액중단당함량적변화,병이용리자색보법대단위질량저물적포도당증가비진행정량분석.실험결과표명:괄의적DILMS침지공예삼수위100℃、8 h、저물목수40(즉직경180~380μm),진일보결합감강화적을이알침지공서(70℃,3 h)이형성적“량보법”예침지가이사단위질량저물중포도당점총환원당적백분비유64.33%상승도96.34%,매해득솔유35.8%상승도83.2%,포도당실제산량제고료1.11배.연구표명감강화적리자액체미유액구유우량적예침지처리효과.
The effects of the composition , impregnation mode and treatment condition of alkali-strengthened DILMS ( Double Ionic Liquid Microemulsion ) on the enzymatic hydrolysis efficiency of eucalyptus were discussed , and the variation of monose content in the residue and the impregnation liquid was analyzed .Moreover , the increment of glucose in the enzymatic hydrolysis process was quantitatively investigated by means of the ion chromatography .Fi-nally, suitable DILMS impregnation conditions , that is, a temperature of 100℃, an impregnation duration of 8 h and a substrate size of 40 meshes ( namely a diameter of 180~380μm) , were determined .Experimental results in-dicate that, by using the alkali-strengthened quadrol (70℃, 3 h) impregnation with the DILMS preimpregnation , the glucose proportion in the total reducing sugar increases from 64.33%to 96.34%, the enzymatic hydrolysis effi-ciency improves from 35.8%to 83.2%, the actual yield of glucose is 2.11 times that of the untreated raw mate-rial.It is thus concluded that the alkali-strengthened DILMS is effective in improving the preimpregnation efficiency .