蚌埠医学院学报
蚌埠醫學院學報
방부의학원학보
ACTA ACADEMIAE MEDICINAE BENGBU
2015年
9期
1244-1246,1247
,共4页
陈少永%陶兆林%张翊%薛洪宝
陳少永%陶兆林%張翊%薛洪寶
진소영%도조림%장익%설홍보
地沟油%微量元素%微波消解%原子吸收光谱法
地溝油%微量元素%微波消解%原子吸收光譜法
지구유%미량원소%미파소해%원자흡수광보법
hogwash oil%trace elements%microwave digestion%atomic absorption spectrometry
目的::探讨地沟油与食用油中5种微量元素之间的差别。方法:选取不同种类的食用油5份和自制猪油1份(均称食用油),收集地沟油和煎炸老油各3份,准确称取各样品0.3~0.4 g,采用微波消解法制成可供测定的溶液,用原子吸收光谱法测定铜(Cu)、锌(Zn)、锰(Mn)、铅(Pb)和铁(Fe)的含量。结果:在实验选定浓度范围内,5种微量元素回收率为97.6%~102.4%,相对标准偏差为0.6%~2.5%。煎炸老油中5种微量元素的含量和大豆油相近;6种食用油中Cu、Zn、Mn和Pb的含量与地沟油差别不大;地沟油和煎炸老油中Fe的含量比6种食用油高(P<0.01)。结论:地沟油中Cu、Zn、Mn、Pb元素含量与食用油的含量差别不大,而Fe元素含量增高,可能因地沟油在炼制、运输过程中与铁制品长期接触有关。
目的::探討地溝油與食用油中5種微量元素之間的差彆。方法:選取不同種類的食用油5份和自製豬油1份(均稱食用油),收集地溝油和煎炸老油各3份,準確稱取各樣品0.3~0.4 g,採用微波消解法製成可供測定的溶液,用原子吸收光譜法測定銅(Cu)、鋅(Zn)、錳(Mn)、鉛(Pb)和鐵(Fe)的含量。結果:在實驗選定濃度範圍內,5種微量元素迴收率為97.6%~102.4%,相對標準偏差為0.6%~2.5%。煎炸老油中5種微量元素的含量和大豆油相近;6種食用油中Cu、Zn、Mn和Pb的含量與地溝油差彆不大;地溝油和煎炸老油中Fe的含量比6種食用油高(P<0.01)。結論:地溝油中Cu、Zn、Mn、Pb元素含量與食用油的含量差彆不大,而Fe元素含量增高,可能因地溝油在煉製、運輸過程中與鐵製品長期接觸有關。
목적::탐토지구유여식용유중5충미량원소지간적차별。방법:선취불동충류적식용유5빈화자제저유1빈(균칭식용유),수집지구유화전작로유각3빈,준학칭취각양품0.3~0.4 g,채용미파소해법제성가공측정적용액,용원자흡수광보법측정동(Cu)、자(Zn)、맹(Mn)、연(Pb)화철(Fe)적함량。결과:재실험선정농도범위내,5충미량원소회수솔위97.6%~102.4%,상대표준편차위0.6%~2.5%。전작로유중5충미량원소적함량화대두유상근;6충식용유중Cu、Zn、Mn화Pb적함량여지구유차별불대;지구유화전작로유중Fe적함량비6충식용유고(P<0.01)。결론:지구유중Cu、Zn、Mn、Pb원소함량여식용유적함량차별불대,이Fe원소함량증고,가능인지구유재련제、운수과정중여철제품장기접촉유관。
Objective:To explore the differences of five kinds of trace elements between edible cooking oil and hogwash oil. Methods:Different kinds of 5 parts edible oil and 1 part homemade lard oil,3 parts old cooking oil and 3 parts hogwash oil were collected. In each sample,0. 3 ~ 0. 4 g was weighed accurately. The samples were digested into a solution for determination by microwave. The contents of copper( Cu) ,zinc( Zn) ,manganese( Mn) ,lead( Pb) and iron( Fe) were determined by atomic absorption spectrometry. Results:In the experimental concentration range,the recovery rate was between 97. 6% to 102. 4%,the relative average deviation was 0. 6% to 2. 5%. The contents of 5 kinds of trace elements in old cooking oil were similar to soybean oil,and there had no differences of Cu,Zn,Mn and Pb contents between the edible oil and hogwash oil,whereas Fe content in old cooking oil and hogwash oil was higher than that in the edible oil(P<0. 01). Conclusions:There had no statistical differences of elements Cu,Zn,Mn and Pb contents between the edible oil and hogwash oil. Fe content was increased in hogwash oil,which may be due to the long-term exposure to the iron products when the hogwash oil was refined and transported.