中国油脂
中國油脂
중국유지
CHINA OILS AND FATS
2015年
8期
8-11
,共4页
张洁%陈功锡%李贵%邢晋
張潔%陳功錫%李貴%邢晉
장길%진공석%리귀%형진
西南山茶%种仁油%超声波辅助提取%气相色谱-质谱法
西南山茶%種仁油%超聲波輔助提取%氣相色譜-質譜法
서남산다%충인유%초성파보조제취%기상색보-질보법
Camellia pitardii%seed kernel oil%ultrasound-assisted extraction%GC-MS
采用超声波辅助提取西南山茶种仁油,研究了超声功率、提取时间、提取温度、料液比对西南山茶种仁油提取率的影响。结果表明,正交实验优化得到的超声波辅助提取西南山茶种仁油的最佳工艺条件为:料液比1∶9,超声功率200 W,提取时间50 min,提取温度55℃;在最佳条件下,西南山茶种仁油提取率为36.74%。气相色谱-质谱分析结果表明,西南山茶种仁油中主要脂肪酸组成为油酸(78.68%)、棕榈酸(8.59%)、十六碳三烯酸(7.92%)、亚油酸(2.43%)、亚麻酸(1.17%)、硬脂酸(0.81%)、花生酸(0.19%),其中不饱和脂肪酸含量高达90.20%,具有较高的应用价值。
採用超聲波輔助提取西南山茶種仁油,研究瞭超聲功率、提取時間、提取溫度、料液比對西南山茶種仁油提取率的影響。結果錶明,正交實驗優化得到的超聲波輔助提取西南山茶種仁油的最佳工藝條件為:料液比1∶9,超聲功率200 W,提取時間50 min,提取溫度55℃;在最佳條件下,西南山茶種仁油提取率為36.74%。氣相色譜-質譜分析結果錶明,西南山茶種仁油中主要脂肪痠組成為油痠(78.68%)、棕櫚痠(8.59%)、十六碳三烯痠(7.92%)、亞油痠(2.43%)、亞痳痠(1.17%)、硬脂痠(0.81%)、花生痠(0.19%),其中不飽和脂肪痠含量高達90.20%,具有較高的應用價值。
채용초성파보조제취서남산다충인유,연구료초성공솔、제취시간、제취온도、료액비대서남산다충인유제취솔적영향。결과표명,정교실험우화득도적초성파보조제취서남산다충인유적최가공예조건위:료액비1∶9,초성공솔200 W,제취시간50 min,제취온도55℃;재최가조건하,서남산다충인유제취솔위36.74%。기상색보-질보분석결과표명,서남산다충인유중주요지방산조성위유산(78.68%)、종려산(8.59%)、십륙탄삼희산(7.92%)、아유산(2.43%)、아마산(1.17%)、경지산(0.81%)、화생산(0.19%),기중불포화지방산함량고체90.20%,구유교고적응용개치。
The kernel oil was obtained from Camellia pitardii seed by ultrasound-assisted extraction,and the effects of ultrasonic power,extraction time,extraction temperature and solid-liquid ratio on extraction rate of Camellia pitardii seed kernel oil were studied. The results showed that the optimal conditions of ultrasound-assisted extraction of Camellia pitardii seed kernel oil were obtained by orthogonal experi-ment as follows:solid-liquid ratio 1∶9,ultrasonic power 200 W,extraction time 50 min,extraction tem-perature 55℃. Under these conditions, the extraction rate of Camellia pitardii seed kernel oil was 36. 74%. The analysis results of GC-MS indicated that the main fatty acid composition of Camellia pi-tardii seed kernel oil was oleic acid (78. 68%), palmitic acid (8. 59%), hexadecatrienoic acid (7. 92%),linoleic acid (2. 43%),linolenic acid (1. 17%),stearic acid (0. 81%) and eicosanoic acid (0. 19%),and the content of unsaturated fatty acids was as high as 90. 20%,which had a high application value.