食品研究与开发
食品研究與開髮
식품연구여개발
FOOD RESEARCH AND CEVELOPMENT
2015年
16期
125-127
,共3页
徐娟%郑志锋%李云仙%雷然
徐娟%鄭誌鋒%李雲仙%雷然
서연%정지봉%리운선%뢰연
电感耦合等离子体发射光谱法%胡萝卜%常微量元素
電感耦閤等離子體髮射光譜法%鬍蘿蔔%常微量元素
전감우합등리자체발사광보법%호라복%상미량원소
ICP-AES%carrot%constant and trace elements
分别采用微波消解法、湿法处理样品,以电感耦合等离子体发射光谱仪(ICP-AES)检测胡萝卜中Cu、Fe、Zn、Mn、Na、K、Ca、Mg、P等16种元素的含量,结果表明:红黄胡萝卜中Fe、Na、K、Ca、Mg、P等元素的含量较高,且K、Mg和Ca表现红胡萝卜>黄胡萝卜,Fe、Na和P表现为黄胡萝卜>红胡萝卜;Sr仅红胡萝卜中含有,含量为26.22μg/g;ICP-AES检测各元素的相对标准偏差(RSD)在0.08%~4.92%之间,各元素回收率在92.18%~106.39%之间。表明湿法消解和微波消解均具有较好的精密度和准确度。
分彆採用微波消解法、濕法處理樣品,以電感耦閤等離子體髮射光譜儀(ICP-AES)檢測鬍蘿蔔中Cu、Fe、Zn、Mn、Na、K、Ca、Mg、P等16種元素的含量,結果錶明:紅黃鬍蘿蔔中Fe、Na、K、Ca、Mg、P等元素的含量較高,且K、Mg和Ca錶現紅鬍蘿蔔>黃鬍蘿蔔,Fe、Na和P錶現為黃鬍蘿蔔>紅鬍蘿蔔;Sr僅紅鬍蘿蔔中含有,含量為26.22μg/g;ICP-AES檢測各元素的相對標準偏差(RSD)在0.08%~4.92%之間,各元素迴收率在92.18%~106.39%之間。錶明濕法消解和微波消解均具有較好的精密度和準確度。
분별채용미파소해법、습법처리양품,이전감우합등리자체발사광보의(ICP-AES)검측호라복중Cu、Fe、Zn、Mn、Na、K、Ca、Mg、P등16충원소적함량,결과표명:홍황호라복중Fe、Na、K、Ca、Mg、P등원소적함량교고,차K、Mg화Ca표현홍호라복>황호라복,Fe、Na화P표현위황호라복>홍호라복;Sr부홍호라복중함유,함량위26.22μg/g;ICP-AES검측각원소적상대표준편차(RSD)재0.08%~4.92%지간,각원소회수솔재92.18%~106.39%지간。표명습법소해화미파소해균구유교호적정밀도화준학도。
The contents of 16 elements such as Cu, Fe, Zn, Mn, Na, K, Ca, Mg and P were studied by ICP-AES with wet digestion method and the microwave digestion in carrots. Results indicated that contents of Fe , Na, K, Ca, Mg and P were higher in both red and yellow carrots. Contents of K, Mg and Ca in red carrots were higher than that in yellow carrots;whereas contents of Fe, Na and P in yellow carrots were higher than that in red carrots. Sr was detected in red carrots and the content was 26.22μg/g. The relative standard deviations and recoveries of all elements determined with ICP-AES were between 0.08%-4.92%and 92.18%-106.39%, respectively. Combination of microwave digestion and wet digestion with the ICP-AES showed that both have better precision and accuracy.