中国医学装备
中國醫學裝備
중국의학장비
CHINA MEDICAL EQUIPMENT
2015年
9期
47-49,50
,共4页
廖建鄂%田莎莎%徐海英%刘明乐%李克荣
廖建鄂%田莎莎%徐海英%劉明樂%李剋榮
료건악%전사사%서해영%류명악%리극영
小型医用蒸馏回收提取锅%研制%应用
小型醫用蒸餾迴收提取鍋%研製%應用
소형의용증류회수제취과%연제%응용
Small medical distillation and recycling pot%Development%Application
目的：研制一种金属制的小型医用蒸馏回收提取锅，以作为1～10 kg药材量的挥发油提取及较低沸点的有机溶媒的回收，并考察其提取挥发油及乙醇回收的效果。方法：自制包括加热、冷凝及收集部分的小型医用提取锅，并考察其提取效果：①将该提取锅分别在直火加热、水蒸汽蒸馏状态下同玻璃提取仪器进行挥发油的提取对照实验；②将该提取锅同玻璃蒸馏器分别用于50%乙醇的回收对照实验。结果：①分别使用研制的蒸馏回收提取锅及玻璃蒸馏器，无论用水蒸汽蒸馏或直火加热提取挥发油时所提取的挥发油数量基本相同，差异无统计学意义；②分别用研制的蒸馏回收提取锅及玻璃蒸馏器进行乙醇回收时，所回收的乙醇量基本相同，差异无统计学意义。结论：小型医用蒸馏回收提取锅可作为1～10 kg药材量的挥发油提取或较低沸点的有机溶媒回收提取用，值得推广。
目的：研製一種金屬製的小型醫用蒸餾迴收提取鍋，以作為1～10 kg藥材量的揮髮油提取及較低沸點的有機溶媒的迴收，併攷察其提取揮髮油及乙醇迴收的效果。方法：自製包括加熱、冷凝及收集部分的小型醫用提取鍋，併攷察其提取效果：①將該提取鍋分彆在直火加熱、水蒸汽蒸餾狀態下同玻璃提取儀器進行揮髮油的提取對照實驗；②將該提取鍋同玻璃蒸餾器分彆用于50%乙醇的迴收對照實驗。結果：①分彆使用研製的蒸餾迴收提取鍋及玻璃蒸餾器，無論用水蒸汽蒸餾或直火加熱提取揮髮油時所提取的揮髮油數量基本相同，差異無統計學意義；②分彆用研製的蒸餾迴收提取鍋及玻璃蒸餾器進行乙醇迴收時，所迴收的乙醇量基本相同，差異無統計學意義。結論：小型醫用蒸餾迴收提取鍋可作為1～10 kg藥材量的揮髮油提取或較低沸點的有機溶媒迴收提取用，值得推廣。
목적：연제일충금속제적소형의용증류회수제취과，이작위1～10 kg약재량적휘발유제취급교저비점적유궤용매적회수，병고찰기제취휘발유급을순회수적효과。방법：자제포괄가열、냉응급수집부분적소형의용제취과，병고찰기제취효과：①장해제취과분별재직화가열、수증기증류상태하동파리제취의기진행휘발유적제취대조실험；②장해제취과동파리증류기분별용우50%을순적회수대조실험。결과：①분별사용연제적증류회수제취과급파리증류기，무론용수증기증류혹직화가열제취휘발유시소제취적휘발유수량기본상동，차이무통계학의의；②분별용연제적증류회수제취과급파리증류기진행을순회수시，소회수적을순량기본상동，차이무통계학의의。결론：소형의용증류회수제취과가작위1～10 kg약재량적휘발유제취혹교저비점적유궤용매회수제취용，치득추엄。
Objective:To develope a kind of small medical distillation and recycling pot for 1~10kg amount of herbs to extract volatile oil and recycle the organic solvents with low boiling point, and examined effect of volatile oil extraction and ethanol recovery effect.Methods: We made a small medical distillation and recycling pot heating, including extraction condensing and collecting part. We examined the following extraction: (1)The small medical distillation and recycling pot and glass extraction apparatus were used to extract volatile oil respectively in a direct fire heating and steam distillation in the control experiments; (2)The small medical distillation and recycling pot and glass extraction apparatus were used to recycle 50% ethanol in the control experiments.Results: (1)In the volatile oil extraction experiments whether direct fire heating or steam distillation, the small medical distillation and recycling pot could extract the essential oil as many as the glass distillation, with no statistical differences. (2)the small medical distillation and recycling pot could recycle ethanol as many as the glass distillation, also with no statistical differences. Conclusion: The small medical distillation and recycling pot could be used for 1~10kg amount of herbs to extract volatile oil and recycle the organic solvents with low boiling point, and worthy recommending.
