河南农业科学
河南農業科學
하남농업과학
JOURNAL OF HENAN AGRICULTURAL SCIENCES
2015年
9期
145-149
,共5页
向福%付建强%胡淇淞%叶莲%倪红成%方元平
嚮福%付建彊%鬍淇淞%葉蓮%倪紅成%方元平
향복%부건강%호기송%협련%예홍성%방원평
大别山松针%松针黄酮%提取工艺%响应面优化
大彆山鬆針%鬆針黃酮%提取工藝%響應麵優化
대별산송침%송침황동%제취공예%향응면우화
pine needles in Dabie Mountains%flavonoid of pine needle%extraction technology%response surface optimization
为探讨松针黄酮的最佳提取工艺,科学开发大别山野生松针资源,采用单因素试验筛选乙醇体积分数、提取时间、提取温度以及料液比等关键影响因素,以总黄酮得率为响应值设计响应面优化试验优化大别山野生松针中黄酮的提取工艺。结果表明,最佳提取工艺为提取温度80℃、提取时间100 min、料液比1∶32(g∶mL)、乙醇体积分数55%,该条件下总黄酮得率可达3.01%,其中料液比对总黄酮得率影响最为显著。
為探討鬆針黃酮的最佳提取工藝,科學開髮大彆山野生鬆針資源,採用單因素試驗篩選乙醇體積分數、提取時間、提取溫度以及料液比等關鍵影響因素,以總黃酮得率為響應值設計響應麵優化試驗優化大彆山野生鬆針中黃酮的提取工藝。結果錶明,最佳提取工藝為提取溫度80℃、提取時間100 min、料液比1∶32(g∶mL)、乙醇體積分數55%,該條件下總黃酮得率可達3.01%,其中料液比對總黃酮得率影響最為顯著。
위탐토송침황동적최가제취공예,과학개발대별산야생송침자원,채용단인소시험사선을순체적분수、제취시간、제취온도이급료액비등관건영향인소,이총황동득솔위향응치설계향응면우화시험우화대별산야생송침중황동적제취공예。결과표명,최가제취공예위제취온도80℃、제취시간100 min、료액비1∶32(g∶mL)、을순체적분수55%,해조건하총황동득솔가체3.01%,기중료액비대총황동득솔영향최위현저。
In order to investigate the extraction technology of flavonoids from pine needles in Dabie Mountains,the effects of key factors,such as ethanol concentration,extraction time,temperature and solid-liquid ratio on the yield of flavonoids were studied based on single factor test,and the extraction technolo-gy was further optimized by response surface optimization test.The optimum extraction technology of fla-vonoids from pine needles was extraction temperature of 80℃,extraction time of 100 min,solid-liquid ra-tio of 1∶32,ethanol concentration of 55%,and solid-liquid ratio had the greatest influence on the yield of flavonoids.Under these conditions,the yield of flavonoids was 3.01%.