周口师范学院学报
週口師範學院學報
주구사범학원학보
Journal of Zhoukou Normal University
2011年
2期
75~77
,共null页
任凯 贾华丽 谢东坡 赵云玲
任凱 賈華麗 謝東坡 趙雲玲
임개 가화려 사동파 조운령
微波消解 火焰原子吸收光谱法 红酒
微波消解 火燄原子吸收光譜法 紅酒
미파소해 화염원자흡수광보법 홍주
microwave digestion; flame atomic absorption spectrometry;red wine
采用空气-乙炔火焰原子吸收光谱法测定红酒中的微量金属元素钙、铁的含量，样品的处理采用微波消解法，钙、铁的吸光度与浓度之间呈线性关系，相关系数分别为0．9982，0．9992，用该法样品加标回收率在95％与105％之间，相对标准偏差小于5％．该方法操作简便、快捷．
採用空氣-乙炔火燄原子吸收光譜法測定紅酒中的微量金屬元素鈣、鐵的含量，樣品的處理採用微波消解法，鈣、鐵的吸光度與濃度之間呈線性關繫，相關繫數分彆為0．9982，0．9992，用該法樣品加標迴收率在95％與105％之間，相對標準偏差小于5％．該方法操作簡便、快捷．
채용공기-을결화염원자흡수광보법측정홍주중적미량금속원소개、철적함량，양품적처리채용미파소해법，개、철적흡광도여농도지간정선성관계，상관계수분별위0．9982，0．9992，용해법양품가표회수솔재95％여105％지간，상대표준편차소우5％．해방법조작간편、쾌첩．
The method for determination of trace metals such as calcium and iron in red wine with air - acetylene flame atomic absorption spectrometry is simple and fast. Samples were dealed with microwave digestion method,the absorption of calcium and their concentration showed a linear relationship. Respectively, their linear correlation coefficients were 0. 9982, 0. 9992. The relative standard deviation was less than 5% and the recovery was from 95% to 105%.
