文物保护与考古科学
文物保護與攷古科學
문물보호여고고과학
Sciences of Conservation and Archaeology
2014年
1期
81~87
,共null页
武望婷 刘树林 楼朋竹 张亦驰 马燕 范胜利 郭斌 任静怡
武望婷 劉樹林 樓朋竹 張亦馳 馬燕 範勝利 郭斌 任靜怡
무망정 류수림 루붕죽 장역치 마연 범성리 곽빈 임정이
装裱 糊化淀粉 粘度 剥离强度
裝裱 糊化澱粉 粘度 剝離彊度
장표 호화정분 점도 박리강도
Mounting ; Gelatinized starch ; Viscosity ; Peeling strength
浆糊是书画装裱过程中主要的黏合材料,是装裱优劣和成败的关键,浆糊的制作条件决定其使用品质。为此,本工作以书画装裱用的粘接剂小麦淀粉为原料,采用快速粘度分析仪(RVA)制作糊化淀粉,研究了不同浓度、搅拌速率、搅拌时间和最高温度等制作条件对糊化曲线的影响。结果表明随着浓度的增加,衰减值和回生值分别增大,说明浆糊的稳定性差、冷却后凝胶性强。随着搅拌时间和速率的增加,最终粘度下降。最高温度对糊化特性曲线形状有影响,最高温度越高,糊化温度升高,最终粘度增大。利用物性仪测试了不同陈化时间对成糊淀粉粘接力的影响。陈化时间越长,糊化淀粉发生大分子链降解或重结晶等不同程度的老化,表现为剥离强度减小,粘附性下降。由实验结果确定浆糊的最优制作条件是浓度3g/25mL,温度95℃,搅拌时间2min,搅拌速度120r/min。以上工作在验证传统经验的同时也给书画装裱提供了理论依据。
漿糊是書畫裝裱過程中主要的黏閤材料,是裝裱優劣和成敗的關鍵,漿糊的製作條件決定其使用品質。為此,本工作以書畫裝裱用的粘接劑小麥澱粉為原料,採用快速粘度分析儀(RVA)製作糊化澱粉,研究瞭不同濃度、攪拌速率、攪拌時間和最高溫度等製作條件對糊化麯線的影響。結果錶明隨著濃度的增加,衰減值和迴生值分彆增大,說明漿糊的穩定性差、冷卻後凝膠性彊。隨著攪拌時間和速率的增加,最終粘度下降。最高溫度對糊化特性麯線形狀有影響,最高溫度越高,糊化溫度升高,最終粘度增大。利用物性儀測試瞭不同陳化時間對成糊澱粉粘接力的影響。陳化時間越長,糊化澱粉髮生大分子鏈降解或重結晶等不同程度的老化,錶現為剝離彊度減小,粘附性下降。由實驗結果確定漿糊的最優製作條件是濃度3g/25mL,溫度95℃,攪拌時間2min,攪拌速度120r/min。以上工作在驗證傳統經驗的同時也給書畫裝裱提供瞭理論依據。
장호시서화장표과정중주요적점합재료,시장표우렬화성패적관건,장호적제작조건결정기사용품질。위차,본공작이서화장표용적점접제소맥정분위원료,채용쾌속점도분석의(RVA)제작호화정분,연구료불동농도、교반속솔、교반시간화최고온도등제작조건대호화곡선적영향。결과표명수착농도적증가,쇠감치화회생치분별증대,설명장호적은정성차、냉각후응효성강。수착교반시간화속솔적증가,최종점도하강。최고온도대호화특성곡선형상유영향,최고온도월고,호화온도승고,최종점도증대。이용물성의측시료불동진화시간대성호정분점접력적영향。진화시간월장,호화정분발생대분자련강해혹중결정등불동정도적노화,표현위박리강도감소,점부성하강。유실험결과학정장호적최우제작조건시농도3g/25mL,온도95℃,교반시간2min,교반속도120r/min。이상공작재험증전통경험적동시야급서화장표제공료이론의거。
In China, paste is the main adhesive material used during the process of painting and calligraphy mount- ing, and is key to determining the quality of mounting and a deciding factor for the success or failure of the whole process. Paste production conditions determine its serviceability. In this study wheat starch was used as the adhe- sive material, a rapid viscosity analyzer (RVA) was used to analyze the adhesive gelatinization curves obtained for pastes made under various conditions of concentration, stirring speed, stirring time and temperature. The results show that as the concentration increases, both the attenuation and retrogradation values increase, indicating poor stability of the paste and strong adhesive power after cooling. As the stirring time and frequency increases, the final viscosity decreases. The highest heating temperature has an effect on the adhesive gelatinization curve: the higher the heating temperature, the higher the gelatinization temperature and the higher the final viscosity. Physical prop- erty test instrument was used to test the influence of different aging times on the viscosity of starch paste. It was found that the longer time the gelatinized starch was kept, the more its macromolecular chains degraded or recrystal- lized and, as a result, the performance of the peel strength decreased, and adhesiveness also declined. Based on this study, it was found that the best conditions for preparing the paste are: paste concentration, 3 g/25 mL; heat- ing temperature, 95°C ; stirring time, 2 minutes; and stirring rate, 12 revolutions/min. This study confirms tradi- tional paste preparation techniques and provides a scientific basis for it.