粮食与油脂
糧食與油脂
양식여유지
Cereals & Oils
2015年
9期
31-35
,共5页
微乳%月见草油%拟三元相图
微乳%月見草油%擬三元相圖
미유%월견초유%의삼원상도
microemulsion%evening primrose oil%pseudo-ternary phase diagram
利用拟三元相图以微乳区面积及乳化效率为指标,考察表面活性剂、有机酸、温度、pH 及盐类对微乳形成能力的影响。结果表明,以吐温80为表面活性剂可以形成无限稀释的水包油型微乳液,直链的月桂酸可使水包油型微乳区面积增大。随着制备温度的升高,微乳形成的速度却明显加快,但温度下降体系的稳定性稍差。在不同 pH 条件下制备微乳时,体系对水的增容量相差很小,说明 pH 对微乳的形成影响很小。低浓度的盐对水的增溶量都有所增加,随着盐浓度的增加,微乳区面积减小。实验确定使用吐温80和月桂酸为复合表面活性剂,在25℃下以滴加水的方法制备水包油型微乳。
利用擬三元相圖以微乳區麵積及乳化效率為指標,攷察錶麵活性劑、有機痠、溫度、pH 及鹽類對微乳形成能力的影響。結果錶明,以吐溫80為錶麵活性劑可以形成無限稀釋的水包油型微乳液,直鏈的月桂痠可使水包油型微乳區麵積增大。隨著製備溫度的升高,微乳形成的速度卻明顯加快,但溫度下降體繫的穩定性稍差。在不同 pH 條件下製備微乳時,體繫對水的增容量相差很小,說明 pH 對微乳的形成影響很小。低濃度的鹽對水的增溶量都有所增加,隨著鹽濃度的增加,微乳區麵積減小。實驗確定使用吐溫80和月桂痠為複閤錶麵活性劑,在25℃下以滴加水的方法製備水包油型微乳。
이용의삼원상도이미유구면적급유화효솔위지표,고찰표면활성제、유궤산、온도、pH 급염류대미유형성능력적영향。결과표명,이토온80위표면활성제가이형성무한희석적수포유형미유액,직련적월계산가사수포유형미유구면적증대。수착제비온도적승고,미유형성적속도각명현가쾌,단온도하강체계적은정성초차。재불동 pH 조건하제비미유시,체계대수적증용량상차흔소,설명 pH 대미유적형성영향흔소。저농도적염대수적증용량도유소증가,수착염농도적증가,미유구면적감소。실험학정사용토온80화월계산위복합표면활성제,재25℃하이적가수적방법제비수포유형미유。
The effects of surfactant,organic acid,temperature,pH and salts on the phase behavior of the microemulsions had been elucidated by pseudo–ternary phase diagram. The results showed that the food–grade O/W microemulsions could formulate from a three–component systems based on water, evening primrose oil and Tween–80. Lauric acid could increase the microemulsion region of oil–in–water. With the increase of temperature for the same formulas,the formation of microemulsions had clearly sped up. But the stability of mieroemulsion became poor with the decrease of temperature. Study on the concentration of salts and pH showed that the microemulsion system had good solubilization of water at low concentration of NaCl and the influence of pH was small. With the increase of NaCl concentration,the microemulsion region became smaller.The O/W microemulsion was prepared by using edible evening primrose oil as the oil–phase,Tween 80 and lauric acid as the surfactant phase at 25 ℃ .