哈尔滨商业大学学报(自然科学版)
哈爾濱商業大學學報(自然科學版)
합이빈상업대학학보(자연과학판)
Journal of Harbin University of Commerce (Natural Sciences Edition)
2015年
4期
389-392
,共4页
张文娓%崔阔%谢明%杨爽爽%宗可昕%范卓文
張文娓%崔闊%謝明%楊爽爽%宗可昕%範卓文
장문미%최활%사명%양상상%종가흔%범탁문
正交试验%萆术硝痛颗粒%尿囊素%挥发油
正交試驗%萆術硝痛顆粒%尿囊素%揮髮油
정교시험%비술초통과립%뇨낭소%휘발유
orthogonal trial%Bixiexiaotong granules%allantoin%essential oil
利用正交试验法,以出膏率、浸出物百分含量、尿囊素及挥发油百分含量为测定指标,研究萆术硝痛颗粒提取工艺中影响因素,并对实验结果进行方差分析.实验结果表明:最佳提取工艺为水提取3次,第1次加水量为处方量的12倍,回流时间为1.5 h,第2次加10倍量水,回流时间为1 h,第3次加8倍量水,回流时间为0.5 h.本实验方法简便易行,稳定可靠,为制剂研究提供实验基础.
利用正交試驗法,以齣膏率、浸齣物百分含量、尿囊素及揮髮油百分含量為測定指標,研究萆術硝痛顆粒提取工藝中影響因素,併對實驗結果進行方差分析.實驗結果錶明:最佳提取工藝為水提取3次,第1次加水量為處方量的12倍,迴流時間為1.5 h,第2次加10倍量水,迴流時間為1 h,第3次加8倍量水,迴流時間為0.5 h.本實驗方法簡便易行,穩定可靠,為製劑研究提供實驗基礎.
이용정교시험법,이출고솔、침출물백분함량、뇨낭소급휘발유백분함량위측정지표,연구비술초통과립제취공예중영향인소,병대실험결과진행방차분석.실험결과표명:최가제취공예위수제취3차,제1차가수량위처방량적12배,회류시간위1.5 h,제2차가10배량수,회류시간위1 h,제3차가8배량수,회류시간위0.5 h.본실험방법간편역행,은정가고,위제제연구제공실험기출.
Orthogonal experimental method was used to test the rate of extraction , the per-centage composition of the extractraction , the allantoin and the essential oil .The influence factors of the extraction process was studied and the experimental results was analysed by ari -ance analysis.The optimal extraction conditions of Bixiexiaotong granules were reflux extrac-tion 3 times.And the first extraction time was 1.5 h with 12 times volumes of water;the sec-ond extraction time was 1 h with 10 times volumes of water;the third extraction time was 0. 5 h with 8 times volumes of water .The optimal extraction technology was easy , accurate and stable , and could provide the experimental basis for the research of preparation .