五邑大学学报(自然科学版)
五邑大學學報(自然科學版)
오읍대학학보(자연과학판)
Journal of Wuyi University(Natural Science Edition)
2015年
3期
16-22
,共7页
射频磁控溅射%涤纶织物%结构色
射頻磁控濺射%滌綸織物%結構色
사빈자공천사%조륜직물%결구색
magnetron sputtering%polyester fabrics%structural colors
采用射频磁控溅射法,在涤纶平纹白坯布上溅射 2SiO 、 2TiO 周期薄膜成功制备出了织物结构色. 利用场发射扫描电镜和超景深三维显微镜对织物结构色的表面形貌和出色效果进行表征,并用分光光度计测量镀膜前后织物的色度差,同时,应用宏观角分辨光谱仪 R1测得织物的多角度反射和散射光谱图,以精确量化描述织物结构色. 通过改变溅射工艺,探究了靶基距、溅射周期、气体流量、工作气压和溅射功率等 5个不同的溅射工艺参数对织物结构色出色效果的影响,结果发现:当靶基距40 mm ,工作气压5 Pa ,气体流量15 sccm ,溅射周期 3个周期以上,溅射功率84 W以上时,织物表面已出色明显,且小范围内调整溅射功率和测射周期对出色效果的影响不大. 靶基距和工作气压对出色效果的影响比较明显,在实验设置的溅射气氛中,工作气压为3 Pa ,靶基距为30 mm时出色效果最好.
採用射頻磁控濺射法,在滌綸平紋白坯佈上濺射 2SiO 、 2TiO 週期薄膜成功製備齣瞭織物結構色. 利用場髮射掃描電鏡和超景深三維顯微鏡對織物結構色的錶麵形貌和齣色效果進行錶徵,併用分光光度計測量鍍膜前後織物的色度差,同時,應用宏觀角分辨光譜儀 R1測得織物的多角度反射和散射光譜圖,以精確量化描述織物結構色. 通過改變濺射工藝,探究瞭靶基距、濺射週期、氣體流量、工作氣壓和濺射功率等 5箇不同的濺射工藝參數對織物結構色齣色效果的影響,結果髮現:噹靶基距40 mm ,工作氣壓5 Pa ,氣體流量15 sccm ,濺射週期 3箇週期以上,濺射功率84 W以上時,織物錶麵已齣色明顯,且小範圍內調整濺射功率和測射週期對齣色效果的影響不大. 靶基距和工作氣壓對齣色效果的影響比較明顯,在實驗設置的濺射氣氛中,工作氣壓為3 Pa ,靶基距為30 mm時齣色效果最好.
채용사빈자공천사법,재조륜평문백배포상천사 2SiO 、 2TiO 주기박막성공제비출료직물결구색. 이용장발사소묘전경화초경심삼유현미경대직물결구색적표면형모화출색효과진행표정,병용분광광도계측량도막전후직물적색도차,동시,응용굉관각분변광보의 R1측득직물적다각도반사화산사광보도,이정학양화묘술직물결구색. 통과개변천사공예,탐구료파기거、천사주기、기체류량、공작기압화천사공솔등 5개불동적천사공예삼수대직물결구색출색효과적영향,결과발현:당파기거40 mm ,공작기압5 Pa ,기체류량15 sccm ,천사주기 3개주기이상,천사공솔84 W이상시,직물표면이출색명현,차소범위내조정천사공솔화측사주기대출색효과적영향불대. 파기거화공작기압대출색효과적영향비교명현,재실험설치적천사기분중,공작기압위3 Pa ,파기거위30 mm시출색효과최호.
Structural colors were fabricated on polyester fabric substrates with periodic films TiO2 and SiO2 by the magnetron sputtering RF method. The morphology of the structural colors on the fabric and surface color effect were characterized by Scanning Electron Microscopy and Ultra-depth 3Dmicroscope. The color differences of the fabric before and after coating were measured with a spectrophotometer. Also the multi-angle reflection and scattered light spectrums were measured by R1 macroscopic angle resolution meters, the fabric structural colors were characterized by precise quantification, and the influence of the five different process parameters (target-substrate distance, sputtering period, gas flow, working gas pressure, and sputtering power) were explored by changing the sputtering technology. The results show that when the target-substrate distance was40mm, working gas pressure5Pa, thegas flow15sccm, the sputtering cycle above 3, and the sputtering power over 84W, the fabric structural color was already obvious, small adjustment of sputtering power and sputtering cycle was of slight influence to the structural color, but the target-substrate distance and working gas pressure had obvious influence on the structural colors, and when the work pressure was set at 3 Pa and the target distance at30mmin the sputtering atmosphere set at the lab, the structural color was the best.