合肥工业大学学报(自然科学版)
閤肥工業大學學報(自然科學版)
합비공업대학학보(자연과학판)
Journal of Hefei University of Technology(Natural Science)
2015年
8期
1040-1044
,共5页
陶磊%李合琴%黄依琴%左敏%柏佩文%陈静武
陶磊%李閤琴%黃依琴%左敏%柏珮文%陳靜武
도뢰%리합금%황의금%좌민%백패문%진정무
钕铁硼%SiC薄膜%射频磁控溅射%耐腐蚀性
釹鐵硼%SiC薄膜%射頻磁控濺射%耐腐蝕性
녀철붕%SiC박막%사빈자공천사%내부식성
NdFeB%SiC thin film%RF magnetron sputtering%corrosion resistance
文章采用射频磁控溅射法在烧结钕铁硼表面沉积SiC薄膜 ,将制备的薄膜分别在200、400 ℃氩气气氛中退火120 min.用X射线衍射仪和原子力显微镜表征薄膜的结构和形貌 ,并研究了镀膜NdFeB在NaCl溶液中的耐腐蚀性能.动电位极化曲线结果表明 ,未镀膜 NdFeB 试样的自腐蚀电流密度为 1.37 × 10-6 A/cm2左右 ,而镀膜未退火试样的自腐蚀电流密度约为1.54 × 10-8 A/cm2 .结果表明 ,在快速且破坏性强的腐蚀情况下 ,镀膜试样抗腐能力比未镀膜好.
文章採用射頻磁控濺射法在燒結釹鐵硼錶麵沉積SiC薄膜 ,將製備的薄膜分彆在200、400 ℃氬氣氣氛中退火120 min.用X射線衍射儀和原子力顯微鏡錶徵薄膜的結構和形貌 ,併研究瞭鍍膜NdFeB在NaCl溶液中的耐腐蝕性能.動電位極化麯線結果錶明 ,未鍍膜 NdFeB 試樣的自腐蝕電流密度為 1.37 × 10-6 A/cm2左右 ,而鍍膜未退火試樣的自腐蝕電流密度約為1.54 × 10-8 A/cm2 .結果錶明 ,在快速且破壞性彊的腐蝕情況下 ,鍍膜試樣抗腐能力比未鍍膜好.
문장채용사빈자공천사법재소결녀철붕표면침적SiC박막 ,장제비적박막분별재200、400 ℃아기기분중퇴화120 min.용X사선연사의화원자력현미경표정박막적결구화형모 ,병연구료도막NdFeB재NaCl용액중적내부식성능.동전위겁화곡선결과표명 ,미도막 NdFeB 시양적자부식전류밀도위 1.37 × 10-6 A/cm2좌우 ,이도막미퇴화시양적자부식전류밀도약위1.54 × 10-8 A/cm2 .결과표명 ,재쾌속차파배성강적부식정황하 ,도막시양항부능력비미도막호.
The SiC thin film was prepared on sintered NdFeB by RF magnetron sputtering .Then they were annealed at 200 ℃ and 400 ℃ for 120 min under argon atmosphere .The structure and morpholo-gy of the SiC thin film were studied by XRD and AFM .The corrosion resistance of the NdFeB speci-men coated with SiC layer in a NaCl solution was also studied .The potentiodynamic polarization curve showed that the corrosion current density of NdFeB was approximately 1.37 × 10-6 A/cm2 ,however the corrosion current density was approximately 1.54 × 10-8 A/cm2 for the NdFeB specimen coated with SiC layer without annealing .The result shows that the NdFeB specimen coated with SiC layer presents better resistance to the fast and destructive corrosion than the bare NdFeB .