中国中医药信息杂志
中國中醫藥信息雜誌
중국중의약신식잡지
Chinese Journal of Information on Traditional Chinese Medicine
2015年
10期
94-96
,共3页
藏药六味木香丸%木香烃内酯%去氢木香内酯%高效液相色谱法
藏藥六味木香汍%木香烴內酯%去氫木香內酯%高效液相色譜法
장약륙미목향환%목향경내지%거경목향내지%고효액상색보법
Tibetan medicineLiuwei Muxiang Pill%Costunolide%Dehydrocostus Lactone%HPLC
目的：建立同时测定藏药六味木香丸中木香烃内酯和去氢木香内酯含量的分析方法。方法采用高效液相色谱法,色谱柱为XDB-C18柱(4.6 mm×50 mm,1.8μm),以甲醇-水(60∶40)为流动相,流速0.8 mL/min,检测波长225 nm。结果藏药六味木香丸中木香烃内酯、去氢木香内酯的线性范围分别为0.2355～1.413μg、0.2913～1.748μg,平均加样回收率分别为99.25%、99.41%。结论该方法准确可靠,结果稳定,重复性好,为评价藏药六味木香丸的质量提供了依据。
目的：建立同時測定藏藥六味木香汍中木香烴內酯和去氫木香內酯含量的分析方法。方法採用高效液相色譜法,色譜柱為XDB-C18柱(4.6 mm×50 mm,1.8μm),以甲醇-水(60∶40)為流動相,流速0.8 mL/min,檢測波長225 nm。結果藏藥六味木香汍中木香烴內酯、去氫木香內酯的線性範圍分彆為0.2355～1.413μg、0.2913～1.748μg,平均加樣迴收率分彆為99.25%、99.41%。結論該方法準確可靠,結果穩定,重複性好,為評價藏藥六味木香汍的質量提供瞭依據。
목적：건립동시측정장약륙미목향환중목향경내지화거경목향내지함량적분석방법。방법채용고효액상색보법,색보주위XDB-C18주(4.6 mm×50 mm,1.8μm),이갑순-수(60∶40)위류동상,류속0.8 mL/min,검측파장225 nm。결과장약륙미목향환중목향경내지、거경목향내지적선성범위분별위0.2355～1.413μg、0.2913～1.748μg,평균가양회수솔분별위99.25%、99.41%。결론해방법준학가고,결과은정,중복성호,위평개장약륙미목향환적질량제공료의거。
Objective To establish the method to analyze the contents of Costunolide and Dehydrocostus Lactone in Tibetan medicineLiuwei Muxiang Pill.Methods HPLC method was used; the XDB-C18 column (4.6 mm × 50 mm, 1.8μm) was adopted;the mobile phase was methanol- water (60∶40);the flow rate was 0.8 mL/min;UV detection was 225 nm.Results The linear range of Costunolide and Dehydrocostus Lactone was 0.235 5-1.413μg and 0.291 3-1.748μg. The average recoveries were 99.25% and 99.41%, respectively.Conclusion The method is accurate, reliable, stable and with good repeatability, which provides the basis for the quality evaluation of Tibetan medicineLiuwei Muxiang Pill.
