工程科学学报
工程科學學報
공정과학학보
Journal of University of Science and Technology Beijing
2015年
9期
1130-1137
,共8页
唐萍%罗琳青%光华%刘江
唐萍%囉琳青%光華%劉江
당평%라림청%광화%류강
微合金钢%连铸%析出行为%模拟%激光共聚焦显微镜
微閤金鋼%連鑄%析齣行為%模擬%激光共聚焦顯微鏡
미합금강%련주%석출행위%모의%격광공취초현미경
micro-alloyed steels%continuous casting%precipitation behaviors%simulation%confocal laser scanning microscopy
通过高温激光共聚焦显微镜模拟了微合金钢在不同冷却工艺下的凝固过程,并原位观察该过程样品表面的变化,探讨样品表面变化与第二相析出的关联性。研究结果表明:随着微合金钢钢液的凝固冷却,样品表面会出现细小浮凸;该浮凸出现的温度及分布位置与第二相的析出理论计算及透射电镜表征结果一致;通过原位观察该浮凸的产生,可间接表征第二相的析出,有利于分析第二相对基体组织演变的影响。
通過高溫激光共聚焦顯微鏡模擬瞭微閤金鋼在不同冷卻工藝下的凝固過程,併原位觀察該過程樣品錶麵的變化,探討樣品錶麵變化與第二相析齣的關聯性。研究結果錶明:隨著微閤金鋼鋼液的凝固冷卻,樣品錶麵會齣現細小浮凸;該浮凸齣現的溫度及分佈位置與第二相的析齣理論計算及透射電鏡錶徵結果一緻;通過原位觀察該浮凸的產生,可間接錶徵第二相的析齣,有利于分析第二相對基體組織縯變的影響。
통과고온격광공취초현미경모의료미합금강재불동냉각공예하적응고과정,병원위관찰해과정양품표면적변화,탐토양품표면변화여제이상석출적관련성。연구결과표명:수착미합금강강액적응고냉각,양품표면회출현세소부철;해부철출현적온도급분포위치여제이상적석출이론계산급투사전경표정결과일치;통과원위관찰해부철적산생,가간접표정제이상적석출,유리우분석제이상대기체조직연변적영향。
Solidification of micro-alloyed steels under different cooling processes was simulated by confocal laser scanning micros-copy ( CLSM) , and the change of the sample surface was in-situ observed. The correlation between the change of the sample surface and the precipitation of secondary phases was discussed. It is found that some small reliefs appear on the sample surface during liquid steel solidification. The appearing temperature and the distribution of reliefs are consistent with the results of the theoretical calculation of secondary phase precipitation and the characterization of transmission electron microscopy ( TEM) . The precipitation of secondary phases can be indirectly characterized by in-situ observations of surface reliefs, which will be helpful to analyze the effect of secondary phases on the evolution of the matrix.