医药导报
醫藥導報
의약도보
Herald of Medicine
2015年
10期
1367-1370
,共4页
金樱子,黔产%多糖%超声提取%星点设计-效应面法
金櫻子,黔產%多糖%超聲提取%星點設計-效應麵法
금앵자,검산%다당%초성제취%성점설계-효응면법
Rosa Laevigatae Michx in Guizhou%Polysaccharides%Ultrasonic extraction%Central composite design-response surface methodology
目的:优化黔产金樱子多糖的超声提取工艺和条件。方法以液料比、提取时间和提取温度为自变量,以黔产金樱子多糖的提取率为因变量,对自变量各水平进行多元线性回归和二项式拟合,采用效应面法优选工艺条件,并进行预测分析。结果黔产金樱子多糖优选工艺:液料比30??1( mL??g),提取时间60 min,提取温度75℃,平均提取率37.54%。结论优化的超声提取工艺和条件简便可靠。
目的:優化黔產金櫻子多糖的超聲提取工藝和條件。方法以液料比、提取時間和提取溫度為自變量,以黔產金櫻子多糖的提取率為因變量,對自變量各水平進行多元線性迴歸和二項式擬閤,採用效應麵法優選工藝條件,併進行預測分析。結果黔產金櫻子多糖優選工藝:液料比30??1( mL??g),提取時間60 min,提取溫度75℃,平均提取率37.54%。結論優化的超聲提取工藝和條件簡便可靠。
목적:우화검산금앵자다당적초성제취공예화조건。방법이액료비、제취시간화제취온도위자변량,이검산금앵자다당적제취솔위인변량,대자변량각수평진행다원선성회귀화이항식의합,채용효응면법우선공예조건,병진행예측분석。결과검산금앵자다당우선공예:액료비30??1( mL??g),제취시간60 min,제취온도75℃,평균제취솔37.54%。결론우화적초성제취공예화조건간편가고。
Objective To select the optimum ultrasonic extracting method of polysaccharides from Rosa Laevigatae Michx in Guizhou. Methods Independent variables were solid-liquid ratio, extraction time and extraction temperature, dependent variable was extraction rate ratio of polysaccharides from Rosa Laevigatae Michx.Linear or nonlinear mathematic models were used to estimate the relationship between independent and dependent variables. Response surface methodology was used to optimize the process of extraction.Prediction was carried out through comparing the observed and predicted value. Results The optimum extraction condition for the polysaccharides was as follows: extracting at 75 ℃ for 60 min and ratio of liquid to solid 30??1 ( mL??g ) . The average extraction yield of polysaccharides was 37. 54% under the optimum extraction condition. Conclusion This optimized extraction process is simple and reliable for the extraction of polysaccharides from Rosa Laevigatae Michx in Guizhou.