理化检验-物理分册
理化檢驗-物理分冊
이화검험-물리분책
Physical Testing and Chemical Analysis Part A:Physical Testing
2015年
10期
711-713,716
,共4页
高炉渣%X射线衍射%K值法%非晶态物质%CaF2标准物质
高爐渣%X射線衍射%K值法%非晶態物質%CaF2標準物質
고로사%X사선연사%K치법%비정태물질%CaF2표준물질
blast furnace slag%X-ray diffraction%K-value method%amorphous phase%CaF2 standard material
首先通过化学分析法和 X 射线衍射法,准确确定高炉渣中的物相组分,然后通过加入标准物质 CaF2,对高炉渣的物相组分进行定量分析,并使用 K 值法计算出非晶态物质的含量。结果表明：采用 X 射线衍射法和 K 值法相结合的方法可以快速准确地测得高炉渣中非晶态物质含量；且标准物质 CaF2的加入质量分数控制在20％时,测定结果更加准确。
首先通過化學分析法和 X 射線衍射法,準確確定高爐渣中的物相組分,然後通過加入標準物質 CaF2,對高爐渣的物相組分進行定量分析,併使用 K 值法計算齣非晶態物質的含量。結果錶明：採用 X 射線衍射法和 K 值法相結閤的方法可以快速準確地測得高爐渣中非晶態物質含量；且標準物質 CaF2的加入質量分數控製在20％時,測定結果更加準確。
수선통과화학분석법화 X 사선연사법,준학학정고로사중적물상조분,연후통과가입표준물질 CaF2,대고로사적물상조분진행정량분석,병사용 K 치법계산출비정태물질적함량。결과표명：채용 X 사선연사법화 K 치법상결합적방법가이쾌속준학지측득고로사중비정태물질함량；차표준물질 CaF2적가입질량분수공제재20％시,측정결과경가준학。
Firstly the phases in blast furnace slag were determined by chemical analysis and X-ray diffraction analysis.And then the content of each phase was quantitatively analyzed by adding standard materials CaF2 and the amorphous content was also calculated by K-value method.The results indicate that the amorphous phase content in blast furnace slag can be quickly and accurately determined by combining X-ray diffraction method and K-value method,and when the standard materials CaF2 addition amount is 20%,more accurate results can be obtained.
