中国药师
中國藥師
중국약사
China Pharmacist
2015年
10期
1718-1720
,共3页
川芎%当归%高效液相色谱法%阿魏酸%原儿茶酸%绿原酸
川芎%噹歸%高效液相色譜法%阿魏痠%原兒茶痠%綠原痠
천궁%당귀%고효액상색보법%아위산%원인다산%록원산
Chuanxiong Rhizoma%Angelicae Sinensis%HPLC%Ferulic acid%Protocatechuic acid%Chlorogenic acid
目的:测定川芎-当归药对水提液中酚类物质含量. 方法:采用离子抑制高效液相色谱法测定川芎-当归药对水提液中阿魏酸、原儿茶酸和绿原酸含量. 结果: 川芎-当归药对中原儿茶酸、阿魏酸和绿原酸分别在0. 90 ~14. 40,1. 25 ~20. 00, 1. 00~16. 00 μg·ml-1范围内与峰面积呈良好线性关系;平均回收率分别为97. 16%、94. 98%、98. 14%(n=9). 结论: 离子抑制高效液相色谱法方法简便、准确、快速、重复性好,可用于川芎-当归药对酚类物质的质量控制.
目的:測定川芎-噹歸藥對水提液中酚類物質含量. 方法:採用離子抑製高效液相色譜法測定川芎-噹歸藥對水提液中阿魏痠、原兒茶痠和綠原痠含量. 結果: 川芎-噹歸藥對中原兒茶痠、阿魏痠和綠原痠分彆在0. 90 ~14. 40,1. 25 ~20. 00, 1. 00~16. 00 μg·ml-1範圍內與峰麵積呈良好線性關繫;平均迴收率分彆為97. 16%、94. 98%、98. 14%(n=9). 結論: 離子抑製高效液相色譜法方法簡便、準確、快速、重複性好,可用于川芎-噹歸藥對酚類物質的質量控製.
목적:측정천궁-당귀약대수제액중분류물질함량. 방법:채용리자억제고효액상색보법측정천궁-당귀약대수제액중아위산、원인다산화록원산함량. 결과: 천궁-당귀약대중원인다산、아위산화록원산분별재0. 90 ~14. 40,1. 25 ~20. 00, 1. 00~16. 00 μg·ml-1범위내여봉면적정량호선성관계;평균회수솔분별위97. 16%、94. 98%、98. 14%(n=9). 결론: 리자억제고효액상색보법방법간편、준학、쾌속、중복성호,가용우천궁-당귀약대분류물질적질량공제.
Objective: To determine the content of phenylpropanoids in the drug pairs of Chuanxiong Rhizoma and Angelicae Sinensis. Methods:An ISC-HPLC method was used to determine the content of ferulic acid, protocatechuic acid and chlorogenic acid. Results:The content of ferulic acid, protocatechuic acid and chlorogenic acid in the drug pairs of Chuanxiong Rhizoma and Angelicae Sinensis all had good linear relationship with the peak area within the range of 0. 90-14. 40,1. 25-20. 00, and 1. 00-16. 00μg·ml-1 , respectively, and the average recovery was 97. 16%, 94. 98% and 98. 14%, respectively (n=9). Conclusion:The HPLC method is simple, rapid, accurate and reproducible, which can be used for the quality control of the drug pairs of Chuanxiong Rhizoma and An-gelicae Sinensis.
