新疆师范大学学报(自然科学版)
新疆師範大學學報(自然科學版)
신강사범대학학보(자연과학판)
Journal of Xinjiang Normal University (Natural Sciences Edition)
2015年
3期
33-38
,共6页
关晓英%乔忠旺%马志深%闫灯周%孙言飞%李锦
關曉英%喬忠旺%馬誌深%閆燈週%孫言飛%李錦
관효영%교충왕%마지심%염등주%손언비%리금
铁酸铋%Co掺杂%溶胶-凝胶法%介电%漏电流
鐵痠鉍%Co摻雜%溶膠-凝膠法%介電%漏電流
철산필%Co참잡%용효-응효법%개전%루전류
BiFeO3%Co-doped%Sol-gel%Dielectric%Leakage current
文章利用溶胶凝胶法在ITO/玻璃衬底上制备不同浓度Co掺杂的BiFe1-x Cox O3( x=0.00、0.05、0.1、0.15)薄膜样品。研究了Co的掺杂对BiFeO 3薄膜的结构、形貌、漏电流及介电性能的影响。 X-射线衍射( XRD)结果显示,未掺的和Co掺杂浓度为5%的BiFeO 3样品为菱方钙钛矿结构,属于R3c空间群。而当Co掺杂浓度为10%和15%时,样品变为四方结构。原子力显微镜( AFM)结果表明,随着Co掺杂浓度的升高,铁酸铋薄膜变得越致密,且尺寸越小。漏电流和介电性能分析结果表明,随着Co元素掺杂浓度的增加,产物的介电损耗有所增加,但其漏电流性能有所下降。当Co的掺杂浓度分别为10%和15%时,薄膜的漏电流很小。
文章利用溶膠凝膠法在ITO/玻璃襯底上製備不同濃度Co摻雜的BiFe1-x Cox O3( x=0.00、0.05、0.1、0.15)薄膜樣品。研究瞭Co的摻雜對BiFeO 3薄膜的結構、形貌、漏電流及介電性能的影響。 X-射線衍射( XRD)結果顯示,未摻的和Co摻雜濃度為5%的BiFeO 3樣品為蔆方鈣鈦礦結構,屬于R3c空間群。而噹Co摻雜濃度為10%和15%時,樣品變為四方結構。原子力顯微鏡( AFM)結果錶明,隨著Co摻雜濃度的升高,鐵痠鉍薄膜變得越緻密,且呎吋越小。漏電流和介電性能分析結果錶明,隨著Co元素摻雜濃度的增加,產物的介電損耗有所增加,但其漏電流性能有所下降。噹Co的摻雜濃度分彆為10%和15%時,薄膜的漏電流很小。
문장이용용효응효법재ITO/파리츤저상제비불동농도Co참잡적BiFe1-x Cox O3( x=0.00、0.05、0.1、0.15)박막양품。연구료Co적참잡대BiFeO 3박막적결구、형모、루전류급개전성능적영향。 X-사선연사( XRD)결과현시,미참적화Co참잡농도위5%적BiFeO 3양품위릉방개태광결구,속우R3c공간군。이당Co참잡농도위10%화15%시,양품변위사방결구。원자력현미경( AFM)결과표명,수착Co참잡농도적승고,철산필박막변득월치밀,차척촌월소。루전류화개전성능분석결과표명,수착Co원소참잡농도적증가,산물적개전손모유소증가,단기루전류성능유소하강。당Co적참잡농도분별위10%화15%시,박막적루전류흔소。
Co-doped BiFe1-xCoxO3(x=0.00、0.05、0.10、0.15) thin films were fabricated on indium tin oxide/glass substrates by sol-gel process.And the structure, morphology and electric properties were studied.X-ray dif-fraction analysis indicated that the pure BiFeO3 and Co-doped 5%BiFeO3 thin films presented single rhombohedral perovskite structure with a space group of R3c.The Co-doped 10%and 15%BiFeO3 thin films presented tetragonal structure with different space symmetry.The atom force microscope ( AFM) indicated thin film become dense and the grains size decreases with Co-doping.Leakage current and dielectric performance analysis results show that with the increase of Co-doping concentration, the product of the dielectric loss increased, but its leakage current per-formance decreased, compared with a pure BiFeO3 film.When the concentration of Co doping was 10%and 15%respectively, the film of the leakage current is very small.