CAJ | 학술논문

从直读光谱仪的光路结构入手，对JJG 768–2005《发射光谱仪》中直读光谱仪部分的波长示值误差、检出限以及重复性和稳定性等检定项目和方法进行了讨论。研究发现，规程存在波长示值误差部分表述不准确、检出限和重复性、稳定性技术指标不详尽等问题。针对上述问题，建议修改“波长示值误差”这一表述，并将其作为后续检定的非必检项；在检出限检定部分对标准物质铁的含量加以要求，并注明元素分析谱线的波长值；对重复性和稳定性选用的标准物质作出元素含量范围的规定，以防造成误判。
종직독광보의적광로결구입수，대JJG 768–2005《발사광보의》중직독광보의부분적파장시치오차、검출한이급중복성화은정성등검정항목화방법진행료토론。연구발현，규정존재파장시치오차부분표술불준학、검출한화중복성、은정성기술지표불상진등문제。침대상술문제，건의수개“파장시치오차”저일표술，병장기작위후속검정적비필검항；재검출한검정부분대표준물질철적함량가이요구，병주명원소분석보선적파장치；대중복성화은정성선용적표준물질작출원소함량범위적규정，이방조성오판。
Several important performance indexes of emission spectrometer were discussed such as indication error of wavelength, detection limit, repeatability and stability via investigating the structure and principle of the monochromator and detector. The research revealed that the definitions of indication error of wavelength was inappropriate, while, some necessary restrictions were not mentioned in terms of detection limit, repeatability and stability. Meanwhile, some suggestions were proposed such as improving the description of wavelength indication error, restricting the purity of reference material as testing the detection limit,repeatability and stability.