化学分析计量
化學分析計量
화학분석계량
Chemical Analysis and Meterage
2015年
5期
88-91
,共4页
孙娟%徐荣%乔丹丹%柏松%杨正标
孫娟%徐榮%喬丹丹%柏鬆%楊正標
손연%서영%교단단%백송%양정표
质量控制图%高锰酸盐指数%饮用水%应用
質量控製圖%高錳痠鹽指數%飲用水%應用
질량공제도%고맹산염지수%음용수%응용
quality control chart%permanganate index%drinking water%application
为确保饮用水中高锰酸盐指数检测结果准确可靠,以GB/T 11892–1989方法《水质高锰酸盐指数的测定》为试验方法,每日对同一质量浓度质控样品平行测定2~3次,统计30组有效数据,通过计算平均值、标准偏差得出上下控制限、警告限和辅助线,绘制出现有实验室人员测试技术水平、试剂、设备、分析方法和环境因素条件下的质量控制图。该质量控制图不仅用于实际检测过程中对检测结果进行监控,还可为实验室的人员分析技能考核、比对监测等分析质量控制行为提供结果判定的依据。
為確保飲用水中高錳痠鹽指數檢測結果準確可靠,以GB/T 11892–1989方法《水質高錳痠鹽指數的測定》為試驗方法,每日對同一質量濃度質控樣品平行測定2~3次,統計30組有效數據,通過計算平均值、標準偏差得齣上下控製限、警告限和輔助線,繪製齣現有實驗室人員測試技術水平、試劑、設備、分析方法和環境因素條件下的質量控製圖。該質量控製圖不僅用于實際檢測過程中對檢測結果進行鑑控,還可為實驗室的人員分析技能攷覈、比對鑑測等分析質量控製行為提供結果判定的依據。
위학보음용수중고맹산염지수검측결과준학가고,이GB/T 11892–1989방법《수질고맹산염지수적측정》위시험방법,매일대동일질량농도질공양품평행측정2~3차,통계30조유효수거,통과계산평균치、표준편차득출상하공제한、경고한화보조선,회제출현유실험실인원측시기술수평、시제、설비、분석방법화배경인소조건하적질량공제도。해질량공제도불부용우실제검측과정중대검측결과진행감공,환가위실험실적인원분석기능고핵、비대감측등분석질량공제행위제공결과판정적의거。
The effective and feasible method was discussed about ensuring the accurate detection result of permanganate index in drinking water. The current national standard Water Quality—Determination of Permanganate Index (GB/T 11892–1989) was used as a detection method. The same quality control sample was determined two or three times everyday, and the effective data of the thirty groups were counted. By calculating the average value and standad deviation of the data, the control limit, boundary limit and auxiliary limit were obtained. With the limits, a quality control chart was outlined, by which the laboratory testing skills, reagents,equipment, analytical methods and environmental factors were taken into account. The chart was not only helpful in controlling the testing results, but also useful in the judgment for quality control activities, such as analysis skills assessment and monitoring comparison.