枣庄学院学报
棘莊學院學報
조장학원학보
Journal of Zaozhuang University
2015年
5期
46-51
,共6页
鞠彩霞%李凤刚%宫亚青%宗志敏%张洪%魏贤勇
鞠綵霞%李鳳剛%宮亞青%宗誌敏%張洪%魏賢勇
국채하%리봉강%궁아청%종지민%장홍%위현용
枣庄煤%甲醇%微波萃取%GC/MS
棘莊煤%甲醇%微波萃取%GC/MS
조장매%갑순%미파췌취%GC/MS
zaozhuangcoal%methanol%microwave extraction%GC/MS
本研究为分析枣庄煤中的有机成分,采用的是甲醇溶剂对枣庄煤进行了微波萃取,并利用GC/MS对萃取物的组成进行了分析。结果表明枣庄煤甲醇萃取物中GC/MS可检测到化合物70种,其中芳香烃占多数,其次是脂肪烃,含杂化合物占少数,含部分其他物质。这可推测枣庄煤样中可能含有的烃类物质为芳香烃、脂肪烃,含氧化合物有酮、吡啶和酸类,还可能有胺类和芳香硝基化合物。
本研究為分析棘莊煤中的有機成分,採用的是甲醇溶劑對棘莊煤進行瞭微波萃取,併利用GC/MS對萃取物的組成進行瞭分析。結果錶明棘莊煤甲醇萃取物中GC/MS可檢測到化閤物70種,其中芳香烴佔多數,其次是脂肪烴,含雜化閤物佔少數,含部分其他物質。這可推測棘莊煤樣中可能含有的烴類物質為芳香烴、脂肪烴,含氧化閤物有酮、吡啶和痠類,還可能有胺類和芳香硝基化閤物。
본연구위분석조장매중적유궤성분,채용적시갑순용제대조장매진행료미파췌취,병이용GC/MS대췌취물적조성진행료분석。결과표명조장매갑순췌취물중GC/MS가검측도화합물70충,기중방향경점다수,기차시지방경,함잡화합물점소수,함부분기타물질。저가추측조장매양중가능함유적경류물질위방향경、지방경,함양화합물유동、필정화산류,환가능유알류화방향초기화합물。
For further analysis of organic components in the zaozhaung coa,this paper introduced that methanol solvent is used to extract by Microwave extraction of zaozhuang coal in Zaozhuang,and the composition of the extracts were analyzed by GC/MS. The results show that 70 new compounds could be detected from Zaozhuang coal by GC/MS,of which aromatic hydrocar-bons are the majority,followed by aliphatic hydrocarbons,hetero compound minority,and some other compounds are part of. The zaozhaung coal was possibly presumed includes the hydrocarbon compounds:the aromatic hydrocarbon,the aliphatic hy-drocarbon,and the oxygen-compounds:ketone ,pyridine and acids but also possibly has the amines and the fragrant nitro compound.